2-Butenedioic acid, 2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl ester

Base Information

Chemical Name:2-Butenedioic acid, 2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl ester
CAS No.:847776-33-4
Molecular Formula:C33H41ClN4O8
Molecular Weight:657.164
Hs Code.:

2-Butenedioic acid,
2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth
oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl
ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Butenedioic acid, 2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl ester

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Technology Process of 2-Butenedioic acid, 2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl ester

There total 1 articles about 2-Butenedioic acid, 2-[[(2S)-2-(3-chlorophenyl)-2-hydroxyethyl]amino]-3-[1-[(1,1-dimethyleth oxy)carbonyl]-4-methyl-6-(4-morpholinyl)-1H-benzimidazol-2-yl]-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 847776-32-3
2-methanesulfonyloxy-3-(1-tert-butyloxycarbonyl-4-methyl-6-morpholin-4-yl-1H-benzoimidazol-2-yl)-but-2-enedioic acid diethyl ester

: 168112-89-8
(S)-(+)-2-amino-1-(3-chlorophenyl)ethanol

: 847776-33-4
(S)-2-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-3-(1-tert-butyloxycarbonyl-4-methyl-6-morpholin-4-yl-1H-benzoimidazol-2-yl)-but-2-enedioic acid diethyl ester

Guidance literature:: In acetonitrile; at 60 ℃; for 1h;

Reference yield: 50.0%

: 847776-33-4
(S)-2-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-3-(1-tert-butyloxycarbonyl-4-methyl-6-morpholin-4-yl-1H-benzoimidazol-2-yl)-but-2-enedioic acid diethyl ester

: (S)-3-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-4-(4-methyl-6-morpholin-4-yl-1H-benzoimidazol-2-yl)-pyrrole-2,5-dione

Guidance literature:: (S)-2-[2-(3-chloro-phenyl)-2-hydroxy-ethylamino]-3-(1-tert-butyloxycarbonyl-4-methyl-6-morpholin-4-yl-1H-benzoimidazol-2-yl)-but-2-enedioic acid diethyl ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

With ammonia; In methanol; dichloromethane; at 50 ℃; for 3h;