5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-

Base Information

Chemical Name:5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-
CAS No.:84142-15-4
Molecular Formula:C₂₀H₂₄N₂
Molecular Weight:292.424
Hs Code.:2933990090
DSSTox Substance ID:DTXSID80233031
Nikkaji Number:J74.740H
Mol file:84142-15-4.mol

Synonyms:84142-15-4;BRN 5579142;5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-;10-(2-(Dimethylamino)ethyl)-5-ethyl-5H-dibenz(b,f)azepine;Dimethyl-N,N ethyl-5 5H-dibenz(b,f)azepine-10-ethanamine [French];Dimethyl-N,N ethyl-5 5H-dibenz(b,f)azepine-10-ethanamine;10-[2-(Dimethylamino)ethyl]-5-ethyl-5H-dibenz[b,f]azepine;DTXSID80233031;LS-60456

Suppliers and Price of 5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-

Chemical Property:

Vapor Pressure:3.16E-07mmHg at 25°C
Boiling Point:418.9°C at 760 mmHg
Flash Point:187.5°C
PSA：6.48000
Density:1.038g/cm³
LogP:4.71530
XLogP3:4.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:292.193948774
Heavy Atom Count:22
Complexity:387

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN1C2=CC=CC=C2C=C(C3=CC=CC=C31)CCN(C)C

Technology Process of 5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl-

There total 5 articles about 5H-Dibenz(b,f)azepine, 10-(2-(dimethylamino)ethyl)-5-ethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 84142-12-1
dihydro-10,11 <(dimethylamino)-2 ethyl>-11 ethyl-5 5H-dibenzazepine-10-ol

: 84142-15-4
dimethyl-N,N ethyl-5 5H-dibenzazepine-10-ethanamine

Guidance literature:: With phosphorus pentoxide; In various solvent(s); for 2.5h; Heating;

Reference yield:

: 19209-60-0
N-acetyl iminostilbene

: 84142-15-4
dimethyl-N,N ethyl-5 5H-dibenzazepine-10-ethanamine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) diborane, 2.) H₂O₂ / 1.) THF, 20 deg C, 1.5 h, 2.) THF-ethanol-water, 0 deg C, 1 h, room temp. overnight

2: 55 percent / CrO₃, H₂SO₄ / acetone; H₂O / 0.5 h / 0 °C

3: 20 percent / ter-BuOK / tetrahydrofuran; hexamethylphosphoric acid triamide / 5 h / 55 °C

4: 90 percent / LiAlH₄ / tetrahydrofuran / 1 h

5: 48 percent / P₂O₅ / various solvent(s) / 2.5 h / Heating

With chromium(VI) oxide; lithium aluminium tetrahydride; sulfuric acid; potassium tert-butylate; dihydrogen peroxide; phosphorus pentoxide; diborane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; water; acetone;

Reference yield:

: 84142-11-0
dihydro-10,11 <(dimethylamino)-2 ethyl>-11 ethyl-5 10H-dibenzazepine-10-one

: 84142-15-4
dimethyl-N,N ethyl-5 5H-dibenzazepine-10-ethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / tetrahydrofuran / 1 h

2: 48 percent / P₂O₅ / various solvent(s) / 2.5 h / Heating

With lithium aluminium tetrahydride; phosphorus pentoxide; In tetrahydrofuran;