3-HydroxyMethyl-3-hydroxypiperidine

Base Information

• Chemical Name: 3-HydroxyMethyl-3-hydroxypiperidine
• CAS No.: 848069-91-0
• Molecular Formula: C6H13NO2
• Molecular Weight: 131.175
• Hs Code.: 2933399090
• Mol file: 848069-91-0.mol

Synonyms:RW2825;QC-2378;3-hydroxymethyl-3-hydroxypiperidine;3-hydroxypiperidin-3-ol;

Chemical Property of 3-HydroxyMethyl-3-hydroxypiperidine

Chemical Property:

• Boiling Point: 270.5±20.0 °C(Predicted)
• PKA: 14.16±0.20(Predicted)
• PSA: 52.49000
• Density: 1.126±0.06 g/cm3(Predicted)
• LogP: -0.57800
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

3-(Hydroxymethyl)-3-piperidinol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-HydroxyMethyl-3-hydroxypiperidine

There total 1 articles about 3-HydroxyMethyl-3-hydroxypiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-hydroxy-3-(hydroxymethyl)-1-(phenylmethyl)piperidine (112197-89-4) → 3-(hydroxymethyl)piperidin-3-ol (848069-91-0)

Guidance literature:

With hydrogen; palladium on carbon; In tetrahydrofuran; methanol; for 20h; under 2585.81 Torr;

Reference yield: 79.0%

3-(hydroxymethyl)piperidin-3-ol (848069-91-0) + 7-chloro-6-fluoro-4-oxo-N-[3,3,4,4,4-pentafluorobutan-2-yl]-1-(2,4,6-trifluorophenyl)-1,4-dihydro-1,8-naphthyridine-3-carboxamide → 6-fluoro-7-[3-hydroxy-3-(hydroxymethyl)piperidin-1-yl]-4-oxo-N-[3,3,4,4,4-pentafluorobutan-2-yl]-1-(2,4,6-trifluorophenyl)-1,4-dihydro-1,8-naphthyridine-3-carboxamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

upstream raw materials:

3-hydroxy-3-(hydroxymethyl)-1-(phenylmethyl)piperidine

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