3-Pyridinecarboxamide, 1,2-dihydro-N-[2-(hydroxyamino)-2-iminoethyl]-6-methyl-5-(1-methyl-1H -pyrazol-5-yl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-

Base Information

• Chemical Name: 3-Pyridinecarboxamide, 1,2-dihydro-N-[2-(hydroxyamino)-2-iminoethyl]-6-methyl-5-(1-methyl-1H -pyrazol-5-yl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-
• CAS No.: 848141-09-3
• Molecular Formula: C20H19F3N6O3
• Molecular Weight: 448.404

Synonyms:

Chemical Property of 3-Pyridinecarboxamide, 1,2-dihydro-N-[2-(hydroxyamino)-2-iminoethyl]-6-methyl-5-(1-methyl-1H -pyrazol-5-yl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-

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Technology Process of 3-Pyridinecarboxamide, 1,2-dihydro-N-[2-(hydroxyamino)-2-iminoethyl]-6-methyl-5-(1-methyl-1H -pyrazol-5-yl)-2-oxo-1-[3-(trifluoromethyl)phenyl]-

There total 1 articles about 3-Pyridinecarboxamide, 1,2-dihydro-N-[2-(hydroxyamino)-2-iminoethyl]-6-methyl-5-(1-methyl-1H -pyrazol-5-yl)-2-oxo-1-[3-(trifluoromethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethyl-phenyl)-1,2-dihydro-pyridine-3-carboxylic acid cyanomethyl amide (848141-08-2) → 6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethylphenyl)-1,2-dihydro-pyridine-3-carboxylic acid(N-hydroxycarbamimidoylmethyl)-amide (848141-09-3)

Guidance literature:

With hydroxylamine hydrochloride; sodium acetate; In ethanol; at 90 ℃; for 3h;

Reference yield: 53.0%

6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethylphenyl)-1,2-dihydro-pyridine-3-carboxylic acid(N-hydroxycarbamimidoylmethyl)-amide (848141-09-3) + orthoformic acid triethyl ester (122-51-0) → 6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethyl-phenyl)-1,2-dihydro-pyridine-3-carboxylic acid([1,2,4]oxadiazol-3-ylmethyl)-amide

Guidance literature:

at 130 ℃; for 3h;

Reference yield:

methylsulphonylacetyl chloride (56841-99-7) + 6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethylphenyl)-1,2-dihydro-pyridine-3-carboxylic acid(N-hydroxycarbamimidoylmethyl)-amide (848141-09-3) → C23H23F3N6O6S

Guidance literature:

In 1,4-dioxane; acetonitrile; at 20 ℃; for 1h;

upstream raw materials:

6-methyl-5-(2-methyl-2H-pyrazol-3-yl)-2-oxo-1-(3-trifluoromethyl-phenyl)-1,2-dihydro-pyridine-3-carboxylic acid cyanomethyl amide

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