2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane

Base Information

Chemical Name:2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane
CAS No.:40632-70-0
Molecular Formula:C12H22O2
Molecular Weight:198.305
Hs Code.:2932999099
European Community (EC) Number:255-014-1
DSSTox Substance ID:DTXSID20193640
Nikkaji Number:J294.722F
Wikidata:Q83066394
Mol file:40632-70-0.mol

Synonyms:2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane;40632-70-0;EINECS 255-014-1;DTXSID20193640;2-Methyl-2-(6-methyl-6-heptenyl)-1,3-dioxolane

Suppliers and Price of 2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane

Chemical Property:

Vapor Pressure:0.043mmHg at 25°C
Boiling Point:246.4°Cat760mmHg
Flash Point:104.6°C
PSA：18.46000
Density:0.898g/cm³
LogP:3.27600
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:198.161979940
Heavy Atom Count:14
Complexity:181

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)CCCCCC1(OCCO1)C

Technology Process of 2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane

There total 5 articles about 2-Methyl-2-(6-methylhept-6-enyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29291-86-9
2-(5-chloro-pentyl)-2-methyl-[1,3]dioxolane

: 40632-70-0
2-methyl-2-(6-methyl-hept-6-enyl)-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone / Heating

2: n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 2 h, 2.) r.t., 4 h

With n-butyllithium; sodium iodide; In tetrahydrofuran; hexane; acetone;
DOI:10.1021/jo00090a041

Reference yield:

: 4630-77-7
7-chloroheptan-2-one

: 40632-70-0
2-methyl-2-(6-methyl-hept-6-enyl)-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / benzene / Heating

2: NaI / acetone / Heating

3: n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 2 h, 2.) r.t., 4 h

With n-butyllithium; toluene-4-sulfonic acid; sodium iodide; In tetrahydrofuran; hexane; acetone; benzene;
DOI:10.1021/jo00090a041

Reference yield:

: 876384-81-5
N'-[6-Chloro-1-methyl-hex-(Z)-ylidene]-N,N-dimethyl-hydrazine

: 40632-70-0
2-methyl-2-(6-methyl-hept-6-enyl)-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 4 steps

1: Amberlyst ion-exchange resin / acetone

2: p-TsOH / benzene / Heating

3: NaI / acetone / Heating

4: n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 2 h, 2.) r.t., 4 h

With n-butyllithium; Amberlyst ion-exchange resin; toluene-4-sulfonic acid; sodium iodide; In tetrahydrofuran; hexane; acetone; benzene;
DOI:10.1021/jo00090a041