Carbamic acid, [(1S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[[1-methyl-5-[(triphenyl methyl)amino]-1H-pyrazol-4-yl]amino]carbonyl]butyl]-, phenylmethyl ester

Base Information

• Chemical Name: Carbamic acid, [(1S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[[1-methyl-5-[(triphenyl methyl)amino]-1H-pyrazol-4-yl]amino]carbonyl]butyl]-, phenylmethyl ester
• CAS No.: 848770-72-9
• Molecular Formula: C41H46N6O5
• Molecular Weight: 702.853

Synonyms:

Chemical Property of Carbamic acid, [(1S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[[1-methyl-5-[(triphenyl methyl)amino]-1H-pyrazol-4-yl]amino]carbonyl]butyl]-, phenylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of Carbamic acid, [(1S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[[1-methyl-5-[(triphenyl methyl)amino]-1H-pyrazol-4-yl]amino]carbonyl]butyl]-, phenylmethyl ester

There total 1 articles about Carbamic acid, [(1S)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[[1-methyl-5-[(triphenyl methyl)amino]-1H-pyrazol-4-yl]amino]carbonyl]butyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzyl 4-tert-butyl {(1S)-1-[(5-amino-1-methyl-1H-pyrazol-4-yl)carbamoyl]tetramethylene}biscarbamate (848770-71-8) + trityl chloride (76-83-5) → 1-benzyl 4-tert-butyl ((1S)-1-{[1-methyl-5-(tritylamino)-1H-pyrazol-4-yl]carbamoyl}tetramethylene) biscarbamate (848770-72-9)

Guidance literature:

With triethylamine; In chloroform; at 20 ℃; for 2h;

Reference yield:

1-benzyl 4-tert-butyl ((1S)-1-{[1-methyl-5-(tritylamino)-1H-pyrazol-4-yl]carbamoyl}tetramethylene) biscarbamate (848770-72-9) → tert-butyl (4S)-4-amino-5-{[1-methyl-5-(tritylamino)-1H-pyrazol-4-yl]amino}-5-oxopentylcarbamate (848770-73-0)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 144h;

upstream raw materials:

1-benzyl 4-tert-butyl {(1S)-1-[(5-amino-1-methyl-1H-pyrazol-4-yl)carbamoyl]tetramethylene}biscarbamate

trityl chloride

Downstream raw materials:

tert-butyl (4S)-4-amino-5-{[1-methyl-5-(tritylamino)-1H-pyrazol-4-yl]amino}-5-oxopentylcarbamate

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