Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato-

Base Information Edit

Chemical Name:Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato-
CAS No.:848776-92-1
Molecular Formula:C12H21NO3S
Molecular Weight:259.37
Hs Code.:
Mol file:848776-92-1.mol

Synonyms:

Suppliers and Price of Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato- Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato-

There total 5 articles about Cyclohexane, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-1-isocyanato- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 848777-77-5
C₁₂H₂₂O₄S

: 848776-92-1
C₁₂H₂₁NO₃S

Guidance literature:: C₁₂H₂₂O₄S; With diphenyl phosphoryl azide; triethylamine; In toluene; at 100 ℃; for 2h;

With sodium hydrogencarbonate; In water; toluene;

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 848776-92-1
C₁₂H₂₁NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 2 h / -10 °C / Industry scale

1.2: -10 - 25 °C

2.1: zinc dibromide / dichloromethane / 1.5 h / 20 - 45 °C / Industry scale

3.1: sodium hydroxide; water / methanol / 16 h / 70 °C / Industry scale

3.2: 10 °C / pH ~ 1.5 / Industry scale

4.1: Oxone / dichloromethane / 24 h / 15 °C / Industry scale

5.1: triethylamine; diphenyl phosphoryl azide / toluene / 9 h / 80 °C / 760.05 Torr / Industry scale; Reflux

With Oxone; n-butyllithium; diphenyl phosphoryl azide; water; triethylamine; diisopropylamine; sodium hydroxide; zinc dibromide; In tetrahydrofuran; methanol; dichloromethane; toluene; 5.1: Curtius Rearrangement;

Reference yield:

: 40195-26-4
1-methoxy-1-trimethylsilyloxymethylenecyclohexane

: 848776-92-1
C₁₂H₂₁NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc dibromide / dichloromethane / 1.5 h / 20 - 45 °C / Industry scale

2.1: sodium hydroxide; water / methanol / 16 h / 70 °C / Industry scale

2.2: 10 °C / pH ~ 1.5 / Industry scale

3.1: Oxone / dichloromethane / 24 h / 15 °C / Industry scale

4.1: triethylamine; diphenyl phosphoryl azide / toluene / 9 h / 80 °C / 760.05 Torr / Industry scale; Reflux

With Oxone; diphenyl phosphoryl azide; water; triethylamine; sodium hydroxide; zinc dibromide; In methanol; dichloromethane; toluene; 4.1: Curtius Rearrangement;