Technology Process of Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]-
There total 4 articles about Cyclohexanecarboxylic acid, 1-[[(1,1-dimethylethyl)sulfonyl]methyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Oxone;
In
dichloromethane;
at 15 ℃;
for 24h;
Industry scale;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: zinc dibromide / dichloromethane / 1.5 h / 20 - 45 °C / Industry scale
2.1: sodium hydroxide; water / methanol / 16 h / 70 °C / Industry scale
2.2: 10 °C / pH ~ 1.5 / Industry scale
3.1: Oxone / dichloromethane / 24 h / 15 °C / Industry scale
With
Oxone; water; sodium hydroxide;
zinc dibromide;
In
methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 2 h / -10 °C / Industry scale
1.2: -10 - 25 °C
2.1: zinc dibromide / dichloromethane / 1.5 h / 20 - 45 °C / Industry scale
3.1: sodium hydroxide; water / methanol / 16 h / 70 °C / Industry scale
3.2: 10 °C / pH ~ 1.5 / Industry scale
4.1: Oxone / dichloromethane / 24 h / 15 °C / Industry scale
With
Oxone; n-butyllithium; water; diisopropylamine; sodium hydroxide;
zinc dibromide;
In
tetrahydrofuran; methanol; dichloromethane;