1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)-

Base Information

Chemical Name:1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)-
CAS No.:848827-39-4
Molecular Formula:C23H31N3O3
Molecular Weight:397.517
Hs Code.:

Synonyms:

Suppliers and Price of 1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)-

There total 10 articles about 1-Nonanol, 2-azido-3,4-bis(phenylmethoxy)-, (2S,3S,4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (R)-1-[(4S,5R)-2,2-Dimethyl-5-((Z)-pent-1-enyl)-[1,3]dioxolan-4-yl]-2-trityloxy-ethanol

: 848827-39-4
(2S,3S,4R)-2-Azido-3,4-bis-benzyloxy-nonan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / hydrogen / palladium(II) hydroxide / ethyl acetate

2: 2,6-lutidine; molecular sieves 4 Angstroem / CH₂Cl₂ / -40 °C

3: tetramethylguanidinium azide / CH₂Cl₂ / -40 - 20 °C

4: 68 percent / acetic acid / methanol / 60 °C

5: pyridine

6: sodium hydride / dimethylformamide

7: acetic acid / H₂O

With pyridine; 2,6-dimethylpyridine; 4 A molecular sieve; hydrogen; sodium hydride; acetic acid; tetramethylguanidinum azide; palladium dihydroxide; In methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 4099-88-1,67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1
(3aS,6R,6aS)-6-(hydroxymethyl)-2,2-dimethyl-tetrahydrofuro[3,4-d]-[1,3]dioxol-4-ol

: 848827-39-4
(2S,3S,4R)-2-Azido-3,4-bis-benzyloxy-nonan-1-ol

Guidance literature:: Multi-step reaction with 9 steps

1.1: pyridine / 6 h / 80 °C

2.1: lithium hexamethyldisilazide / tetrahydrofuran / 0 °C

2.2: 85 percent / lithium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

3.1: 88 percent / hydrogen / palladium(II) hydroxide / ethyl acetate

4.1: 2,6-lutidine; molecular sieves 4 Angstroem / CH₂Cl₂ / -40 °C

5.1: tetramethylguanidinium azide / CH₂Cl₂ / -40 - 20 °C

6.1: 68 percent / acetic acid / methanol / 60 °C

7.1: pyridine

8.1: sodium hydride / dimethylformamide

9.1: acetic acid / H₂O

With pyridine; 2,6-dimethylpyridine; 4 A molecular sieve; hydrogen; sodium hydride; acetic acid; tetramethylguanidinum azide; lithium hexamethyldisilazane; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 2.2: Wittig reaction;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-lyxose

: 848827-39-4
(2S,3S,4R)-2-Azido-3,4-bis-benzyloxy-nonan-1-ol

Guidance literature:: Multi-step reaction with 10 steps

1.1: camphorsulfonic acid

2.1: pyridine / 6 h / 80 °C

3.1: lithium hexamethyldisilazide / tetrahydrofuran / 0 °C

3.2: 85 percent / lithium hexamethyldisilazide / tetrahydrofuran / 0 - 20 °C

4.1: 88 percent / hydrogen / palladium(II) hydroxide / ethyl acetate

5.1: 2,6-lutidine; molecular sieves 4 Angstroem / CH₂Cl₂ / -40 °C

6.1: tetramethylguanidinium azide / CH₂Cl₂ / -40 - 20 °C

7.1: 68 percent / acetic acid / methanol / 60 °C

8.1: pyridine

9.1: sodium hydride / dimethylformamide

10.1: acetic acid / H₂O

With pyridine; 2,6-dimethylpyridine; 4 A molecular sieve; camphor-10-sulfonic acid; hydrogen; sodium hydride; acetic acid; tetramethylguanidinum azide; lithium hexamethyldisilazane; palladium dihydroxide; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; 3.2: Wittig reaction;
DOI:10.1016/j.tet.2004.12.027