2'-deoxyguanosine 3'-(dihydrogen phosphate)

Base Information

• Chemical Name: 2'-deoxyguanosine 3'-(dihydrogen phosphate)
• CAS No.: 6220-62-8
• Molecular Formula: C10H14 N5 O7 P
• Molecular Weight: 347.224
• Mol file: 6220-62-8.mol

Synonyms:Guanosine,2'-deoxy-, 3'-(dihydrogen phosphate) (8CI); Guanosine, 2'-deoxy-, 3'-phosphate(7CI); 2'-Deoxy-3'-guanylic acid; 2'-Deoxyguanosine 3'-monophosphate;2'-Deoxyguanosine 3'-phosphate; 3'-dGMP; Deoxyguanosine 3'-monophosphate;Deoxyguanosine 3'-phosphate; dGp

Chemical Property of 2'-deoxyguanosine 3'-(dihydrogen phosphate)

Chemical Property:

• PSA: 195.62000
• LogP: -0.95930

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2'-deoxyguanosine 3'-(dihydrogen phosphate)

There total 20 articles about 2'-deoxyguanosine 3'-(dihydrogen phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C49H62N23O28P5 + C10H15N5O10P2*C6H15N → 2'-deoxyguanosine-3'-monophosphate (6220-62-8)

Guidance literature:

C₄₉H₆₂N₂₃O₂₈P₅; With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; at 17 ℃; for 48h; pH=6;

C₁₀H₁₅N₅O₁₀P₂*C₆H₁₅N; With DL-dithiothreitol; ATP; manganese(ll) chloride; Spermine; at 48 ℃; for 17h; pH=8;

With alkaline phosphatase; at 37 ℃; for 1h; pH=8; Further stages.;

DOI:10.1021/ol990240n

Reference yield:

Phosphoric acid mono-[(2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-3-yl] ester → 2'-deoxyguanosine-3'-monophosphate (6220-62-8)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 1h; Yield given;

DOI:10.1016/S0040-4039(00)96095-7

Reference yield:

Phosphoric acid mono-[(2R,3S,5R)-2-hydroxymethyl-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yl] ester → 2'-deoxyguanosine-3'-monophosphate (6220-62-8)

Guidance literature:

With ammonium hydroxide; In water; at 65 ℃; for 6h;

DOI:10.1016/S0040-4039(00)01251-X

upstream raw materials:

Phosphoric acid mono-[(2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-tetrahydro-furan-3-yl] ester

5'-O-dimethoxytrityl-N-isobutyryldeoxyguanosine

Phosphoric acid diallyl ester (2R,3S,5R)-5-(2-amino-6-oxo-1,6-dihydro-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-3-yl ester

2’-deoxy-5’-O-tert-butyldimethylsilylguanosine

Downstream raw materials:

2'-Deoxyguanosine

N-(3'-monophosphate-2'-deoxyguanosin-8-yl)-4-methylaniline

Phosphoric acid mono-[(2R,3S,5R)-5-(2-amino-6-oxo-8-m-tolylamino-1,6-dihydro-purin-9-yl)-2-hydroxymethyl-tetrahydro-furan-3-yl] ester

Phosphoric acid mono-{(2R,3S,5R)-5-[2-amino-8-(2,4-dimethyl-phenylamino)-6-oxo-1,6-dihydro-purin-9-yl]-2-hydroxymethyl-tetrahydro-furan-3-yl} ester

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