Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane

Base Information

Chemical Name:Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane
CAS No.:84904-72-3
Molecular Formula:C20H17OPS
Molecular Weight:336.394
Hs Code.:
DSSTox Substance ID:DTXSID10510044
Nikkaji Number:J1.421.472K
Wikidata:Q82368065

Synonyms:84904-72-3;DTXSID10510044;Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:336.07377333
Heavy Atom Count:23
Complexity:407

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(P(=O)(C1=CC=CC=C1)C2=CC=CC=C2)SC3=CC=CC=C3

Technology Process of Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane

There total 6 articles about Oxo(diphenyl)[1-(phenylsulfanyl)ethenyl]-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 84904-73-4
1-chloro-1-phenylthioethyl-diphenylphosphine oxide

: 31238-57-0
diphenyl(phenylthiomethyl)phosphine oxide

: 84904-72-3
Diphenyl (1-phenylthiovinyl)phosphine oxide

Guidance literature:: With silica gel; In ethyl acetate; for 16h;
DOI:10.1016/S0040-4039(00)88377-X

Reference yield: 65.0%

: 84904-74-5
1-phenylsulphinylethyldiphenylphosphine oxide

: 84904-72-3
Diphenyl (1-phenylthiovinyl)phosphine oxide

Guidance literature:: With methanesulfonic acid; acetic anhydride; In dichloromethane; at 25 ℃; for 192h;
DOI:10.1016/S0040-4039(00)88377-X

Reference yield:

: 66164-48-5
diphenyl(1-(phenylthio)ethyl)phosphine oxide

: 84904-72-3
Diphenyl (1-phenylthiovinyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / MCPBA / CH₂Cl₂; tetrahydrofuran / 1 h / -78 °C

2: 65 percent / Ac₂O, MeSO₃H / CH₂Cl₂ / 192 h / Ambient temperature

With methanesulfonic acid; acetic anhydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;