Carbamic acid, [2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-, 1,1-dimethylethyl ester
CAS No.:849100-80-7
Molecular Formula:C50H66N6O13
Molecular Weight:959.106
Hs Code.:

Carbamic acid,
[2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro
phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-,
1,1-dimethylethyl ester

Synonyms:

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Chemical Property of Carbamic acid, [2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-, 1,1-dimethylethyl ester

There total 6 articles about Carbamic acid, [2-[3-acetyl-5-[2-[[3-[[12-[(4-nitrophenyl)amino]dodecyl]oxy]-5-[2-[(4-nitro phenyl)amino]ethoxy]benzoyl]amino]ethoxy]phenoxy]ethyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3-(2-amino-ethoxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester; hydrochloride

: 849100-73-8
3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoic acid

: 849100-80-7
3-(2-tert-butoxycarbonylamino-ethoxy)-5-(2-{3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoylamino}-ethoxy)-benzoic acid methyl ester

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1002/ejoc.200400609

Reference yield:

: 849100-67-0
3-hydroxy-5-[2-(Boc-amino)ethoxy]benzoic acid methylester

: 849100-80-7
3-(2-tert-butoxycarbonylamino-ethoxy)-5-(2-{3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoylamino}-ethoxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / potassium carbonate / dimethylformamide / 40 °C

2: 100 percent / hydrogen / Pd/C / ethanol; CHCl₃ / 2250.18 Torr

3: 78 percent / BOP; DiPEA / CH₂Cl₂ / 1 h / 20 °C

With hydrogen; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.200400609

Reference yield:

: 849100-79-4
3-(2-benzyloxycarbonylamino-ethoxy)-5-(2-tert-butoxycarbonylamino-ethoxy)-benzoic acid methyl ester

: 849100-80-7
3-(2-tert-butoxycarbonylamino-ethoxy)-5-(2-{3-[12-(4-nitro-phenylamino)-dodecyloxy]-5-[2-(4-nitro-phenylamino)-ethoxy]-benzoylamino}-ethoxy)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / hydrogen / Pd/C / ethanol; CHCl₃ / 2250.18 Torr

2: 78 percent / BOP; DiPEA / CH₂Cl₂ / 1 h / 20 °C

With hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; dichloromethane; chloroform;
DOI:10.1002/ejoc.200400609