Carbamic acid, [(1S,2S,4S)-2-hydroxy-5-methyl-4-[[[(1S)-1-methyl-2-oxo-2-[(phenylmeth yl)amino]ethyl]amino]carbonyl]-1-(2-methylpropyl)hexyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: Carbamic acid, [(1S,2S,4S)-2-hydroxy-5-methyl-4-[[[(1S)-1-methyl-2-oxo-2-[(phenylmeth yl)amino]ethyl]amino]carbonyl]-1-(2-methylpropyl)hexyl]-, 1,1-dimethylethyl ester
• CAS No.: 849410-38-4
• Molecular Formula: C27H45N3O5
• Molecular Weight: 491.671

Synonyms:

Chemical Property of Carbamic acid, [(1S,2S,4S)-2-hydroxy-5-methyl-4-[[[(1S)-1-methyl-2-oxo-2-[(phenylmeth yl)amino]ethyl]amino]carbonyl]-1-(2-methylpropyl)hexyl]-, 1,1-dimethylethyl ester

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Technology Process of Carbamic acid, [(1S,2S,4S)-2-hydroxy-5-methyl-4-[[[(1S)-1-methyl-2-oxo-2-[(phenylmeth yl)amino]ethyl]amino]carbonyl]-1-(2-methylpropyl)hexyl]-, 1,1-dimethylethyl ester

There total 1 articles about Carbamic acid, [(1S,2S,4S)-2-hydroxy-5-methyl-4-[[[(1S)-1-methyl-2-oxo-2-[(phenylmeth yl)amino]ethyl]amino]carbonyl]-1-(2-methylpropyl)hexyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

→ tert-butyl (1S,2S,4S)-4-({[(1S)-2-(benzylamino)-1-methyl-2-oxoethyl]amino}carbonyl)-2-hydroxy-1-isobutyl-5-methylhexylcarbamate (849410-38-4)

Guidance literature:

Reference yield: 71.0%

3-[(benzylsulfonyl)(methyl)amino]benzoic acid (849410-18-0) + tert-butyl (1S,2S,4S)-4-({[(1S)-2-(benzylamino)-1-methyl-2-oxoethyl]amino}carbonyl)-2-hydroxy-1-isobutyl-5-methylhexylcarbamate (849410-38-4) → N-[(1S,2S,4S)-4-({[(1S)-2-(benzylamino)-1-methyl-2-oxoethyl]amino}carbonyl)-2-hydroxy-1-isobutyl-5-methylhexyl]-3-[(benzylsulfonyl)(methyl)amino]benzamide

Guidance literature:

tert-butyl (1S,2S,4S)-4-({[(1S)-2-(benzylamino)-1-methyl-2-oxoethyl]amino}carbonyl)-2-hydroxy-1-isobutyl-5-methylhexylcarbamate; With trifluoroacetic acid; In dichloromethane; for 0.5h;

3-[(benzylsulfonyl)(methyl)amino]benzoic acid; With N-ethyl-N,N-diisopropylamine; HATU; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 4h;

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