2-CYCLOHEXYLACETALDEHYDE

Base Information

• Chemical Name: 2-CYCLOHEXYLACETALDEHYDE
• CAS No.: 5664-21-1
• Molecular Formula: C8H14 O
• Molecular Weight: 126.199
• Hs Code.: 2912299000
• Mol file: 5664-21-1.mol

Synonyms:2-Cyclohexylacetaldehyde;Cyclohexylacetaldehyde; Cyclohexylmethyl carboxaldehyde; NSC 244934

Chemical Property of 2-CYCLOHEXYLACETALDEHYDE

Chemical Property:

• Vapor Pressure: 0.568mmHg at 25°C
• Boiling Point: 189.5°Cat760mmHg
• Flash Point: 61.9°C
• PSA: 17.07000
• Density: 0.892g/cm³
• LogP: 2.15570
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C
• Solubility.: Chloroform (Sparingly)

Purity/Quality:

97% ^*data from raw suppliers

Cyclohexylacetaldehyde(~90%) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CYCLOHEXYLACETALDEHYDE

There total 48 articles about 2-CYCLOHEXYLACETALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

cyclohexylethan-1-ol (4442-79-9) → cyclohexylacetaldehyde (5664-21-1)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 3h;

Reference yield: 100.0%

2-cyclohexylidene ethanol (932-89-8) → cyclohexylacetaldehyde (5664-21-1)

Guidance literature:

With (1,5-cyclooctadiene)(pyridine)(tricyclohexylphosphine)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; hydrogen; In tetrahydrofuran; at 23 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2009.04.130

Reference yield: 97.0%

methyl cyclohexylacetate (14352-61-5) → cyclohexylacetaldehyde (5664-21-1)

Guidance literature:

methyl cyclohexylacetate; With diisobutylaluminium hydride; In dichloromethane; at -70 ℃; for 5h;

With water; ammonium chloride; In dichloromethane;

upstream raw materials:

cyclohexylethan-1-ol

1-Cyclohexyl-2,2-diethoxyethan

(2,2-dichloro-ethyl)-cyclohexane

2-ethoxy-1-cyclohexyl-ethanol

Downstream raw materials:

4-cyclohexyl-trans-crotonic acid

cyclohexyl-acetaldehyde-(2,4-dinitro-phenylhydrazone)

N-(4-Methoxyphenyl)cyclohexylacetaldimine

ethyl 4-cyclohexyl-3-hydroxy-2,2-dimethylbutanoate