6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one

Base Information

Chemical Name:6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one
CAS No.:16964-48-0
Molecular Formula:C₂₀H₂₈O₃
Molecular Weight:316.441
Hs Code.:
DSSTox Substance ID:DTXSID30937658
Mol file:16964-48-0.mol

Synonyms:6a,7,10,10a-tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one;6a,7,10,10a-tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one, (+)-isomer;6a,7,10,10a-tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one, (-)-isomer;THC-9-one

Suppliers and Price of 6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one

Chemical Property:

Vapor Pressure:1.57E-07mmHg at 25°C
Boiling Point:416.5°Cat760mmHg
Flash Point:139.7°C
PSA：46.53000
Density:1.072g/cm³
LogP:4.74870
XLogP3:5.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:316.20384475
Heavy Atom Count:23
Complexity:431

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCC1=CC(=C2C3CC(=O)CCC3C(OC2=C1)(C)C)O

Technology Process of 6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one

There total 4 articles about 6a,7,10,10a-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo(b,d)pyran-9(8H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 6616-69-9,16964-48-0,16964-51-5,52195-11-6,60761-09-3,63790-37-4,138383-58-1
11-nor-9-keto-6a,10a-cis-HHC

: 6616-69-9,16964-48-0,16964-51-5,52195-11-6,60761-09-3,63790-37-4,138383-58-1
dl-6aα,7,10,10aα-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo[b,d]pyran-9(8H)-on

Guidance literature:: With aluminium trichloride; In dichloromethane; for 5h; Ambient temperature;
DOI:10.1139/v82-403

Reference yield: 24.0%

: 61597-37-3
4-(1-hydroxy-1-methylethyl)-1-methoxy-1,4-cyclohexadiene

: 500-66-3
Olivetol

: 6616-69-9,16964-48-0,16964-51-5,52195-11-6,60761-09-3,63790-37-4,138383-58-1
11-nor-9-keto-6a,10a-cis-HHC

Guidance literature:: With water; tin(IV) chloride; In dichloromethane; at 0 ℃; for 7h;
DOI:10.1139/v82-403

Reference yield:

: 61597-37-3
4-(1-hydroxy-1-methylethyl)-1-methoxy-1,4-cyclohexadiene

: 6616-69-9,16964-48-0,16964-51-5,52195-11-6,60761-09-3,63790-37-4,138383-58-1
dl-6aα,7,10,10aα-Tetrahydro-1-hydroxy-6,6-dimethyl-3-pentyl-6H-dibenzo[b,d]pyran-9(8H)-on

Guidance literature:: Multi-step reaction with 2 steps

1: 24 percent / water, stannic chloride / CH₂Cl₂ / 7 h / 0 °C

2: 58 percent / aluminium chloride / CH₂Cl₂ / 5 h / Ambient temperature

With aluminium trichloride; water; tin(IV) chloride; In dichloromethane;
DOI:10.1139/v82-403