ARP 101

Base Information

Chemical Name:ARP 101
CAS No.:849773-63-3
Molecular Formula:C₂₀H₂₆N₂O₅S
Molecular Weight:406.503
Hs Code.:
Mol file:849773-63-3.mol

Synonyms:ARP 101;

Suppliers and Price of ARP 101

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
ARP 101
5mg
$ 180.00

ApexBio Technology
ARP 101
5mg
$ 282.00

Total 6 raw suppliers

Chemical Property of ARP 101

Chemical Property:

PSA：104.32000
LogP:4.68600
Solubility.:<40.65mg/ml in DMSO; <10.16mg/ml in ethanol

Purity/Quality:

99%, ^*data from raw suppliers

ARP 101 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ARP 101

There total 9 articles about ARP 101 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 849773-59-7
(R)-N-(tert-butyldimethylsilyloxy)-2-(N-isopropoxybiphenyl-4-ylsulfonamido)-3-methylbutanamide

: 849773-63-3,849773-64-4
ARP101

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 5h;
DOI:10.1016/j.bmc.2006.01.056

Reference yield:

: 704888-95-9
N-isopropoxy-1,1'-biphenyl-4-sulfonamide

: 849773-63-3,849773-64-4
ARP101

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate; tetrabutylammonium hydrogen sulfate / dimethylformamide / 3 h / 20 °C

2: 30 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 20 h / 20 °C

3: 48 percent / trifluoroacetic acid / CH₂Cl₂ / 5 h / 0 °C

With tetra(n-butyl)ammonium hydrogensulfate; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.01.056

Reference yield:

: 17407-55-5
(S)-2-Hydroxy-3-methylbutanoic acid

: 849773-63-3,849773-64-4
ARP101

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / 18 h / 20 °C

2: toluene / 3 h / 95 °C

3: LiOH / H₂O; methanol; tetrahydrofuran / 3 h / 20 °C

4: 53 percent / diethyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 5 h / 0 °C

5: 30 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂ / 20 h / 20 °C

6: 48 percent / trifluoroacetic acid / CH₂Cl₂ / 5 h / 0 °C

With lithium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 4: Mitsunobu reaction;
DOI:10.1016/j.bmc.2006.01.056