4a,5-dihydrofluorantheno[2,3-b]oxirene-5,5a(3bH)-diol

Base Information

Chemical Name:4a,5-dihydrofluorantheno[2,3-b]oxirene-5,5a(3bH)-diol
CAS No.:83349-68-2
Molecular Formula:C₁₆H₁₂O₃
Molecular Weight:252.269
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4a,5-dihydrofluorantheno[2,3-b]oxirene-5,5a(3bH)-diol

Chemical Property:

Vapor Pressure:7.31E-11mmHg at 25°C
Boiling Point:501.1°Cat760mmHg
Flash Point:256.9°C
PSA：52.99000
Density:1.591g/cm³
LogP:1.71730

Purity/Quality:

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Technology Process of 4a,5-dihydrofluorantheno[2,3-b]oxirene-5,5a(3bH)-diol

There total 3 articles about 4a,5-dihydrofluorantheno[2,3-b]oxirene-5,5a(3bH)-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 83291-55-8
C₁₉H₂₀O₃Si

: 83349-68-2
C₁₆H₁₂O₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.166667h;
DOI:10.1021/jo00146a011

Reference yield:

: 83291-52-5,83291-53-6
(1S,10bS)-10b-Trimethylsilanyloxy-1,10b-dihydro-fluoranthen-1-ol

: 83349-68-2
C₁₆H₁₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 6.5 M t-BuOOH in CH₂Cl₂, VO(acac)2 / benzene / 1 h / Ambient temperature

2: 100 percent / 1 M n-Bu₄NF / tetrahydrofuran / 0.17 h / 0 °C

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; In tetrahydrofuran; benzene;
DOI:10.1021/jo00146a011

Reference yield:

: 83291-51-4
(2S,10bS)-2-Phenylselanyl-10b-trimethylsilanyloxy-1,2,3,10b-tetrahydro-fluoranthen-1-ol

: 83349-68-2
C₁₆H₁₂O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / 30percent H₂O₂ / tetrahydrofuran / 1.5 h / 0 °C

2: 100 percent / 6.5 M t-BuOOH in CH₂Cl₂, VO(acac)2 / benzene / 1 h / Ambient temperature

3: 100 percent / 1 M n-Bu₄NF / tetrahydrofuran / 0.17 h / 0 °C

With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; dihydrogen peroxide; In tetrahydrofuran; benzene;
DOI:10.1021/jo00146a011