rubroflavin

Base Information

Chemical Name:rubroflavin
CAS No.:138749-63-0
Molecular Formula:C9H11 N3 O3 S2
Molecular Weight:273.33194
Hs Code.:
Mol file:138749-63-0.mol

Synonyms:Hydrazinecarboxamide,2-[2-(methylsulfinyl)-6-(methylthio)-4-oxo-2,5-cyclohexadien-1-ylidene]-,[S-(Z)]-; (-)-(S)-Rubroflavin; Rubroflavin

Suppliers and Price of rubroflavin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of rubroflavin

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：147.12000
Density:1.59g/cm³
LogP:1.87310

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of rubroflavin

There total 5 articles about rubroflavin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: deoxyrubroflavin

: 138749-63-0
rubroflavin

Guidance literature:: Multi-step reaction with 3 steps

1.1: 88 percent / dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / dimethylformamide / 0.75 h / 0 - 20 °C

2.1: Ti(OiPr)4; (2S,3S)-DET; water / CH₂Cl₂ / -20 °C

2.2: TBHP / toluene / -20 °C

2.3: CCl₄ / repeated recrystallization

3.1: aq. NaOH / methanol

With titanium(IV) isopropylate; dmap; sodium hydroxide; diethyl (2S,3S)-tartrate; water; dicyclohexyl-carbodiimide; In methanol; dichloromethane; N,N-dimethyl-formamide; 2.1: Kagan's procedure;
DOI:10.1002/1099-0690(200108)2001:16<3097::AID-EJOC3097>3.0.CO;2-V