Benzeneethanimidamide, N-hydroxy-4-(tetradecylthio)-

Base Information

Chemical Name:Benzeneethanimidamide, N-hydroxy-4-(tetradecylthio)-
CAS No.:850143-39-4
Molecular Formula:C22H38N2OS
Molecular Weight:378.623
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneethanimidamide, N-hydroxy-4-(tetradecylthio)-

Chemical Property:

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Technology Process of Benzeneethanimidamide, N-hydroxy-4-(tetradecylthio)-

There total 4 articles about Benzeneethanimidamide, N-hydroxy-4-(tetradecylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 850143-16-7
1-bromomethyl-4-tetradecylsulfanyl-benzene

: 850143-39-4
4-(tetradecylthio)phenylacetamidoxime

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / dimethylformamide / 48 h / 20 °C

2: 51 percent / hydroxylamine hydrochloride; K₂CO₃ / ethanol / 18 h / Heating

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016

Reference yield:

: 112-71-0
1-Bromotetradecane

: 850143-39-4
4-(tetradecylthio)phenylacetamidoxime

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / NaOH / ethanol; dimethylformamide / 20 °C

2: 68 percent / HBr; acetic acid / 30 h / 20 °C

3: 100 percent / dimethylformamide / 48 h / 20 °C

4: 51 percent / hydroxylamine hydrochloride; K₂CO₃ / ethanol / 18 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; hydrogen bromide; potassium carbonate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016

Reference yield:

: 94763-48-1
phenyl tetradecyl thioether

: 850143-39-4
4-(tetradecylthio)phenylacetamidoxime

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / HBr; acetic acid / 30 h / 20 °C

2: 100 percent / dimethylformamide / 48 h / 20 °C

3: 51 percent / hydroxylamine hydrochloride; K₂CO₃ / ethanol / 18 h / Heating

With hydroxylamine hydrochloride; hydrogen bromide; potassium carbonate; acetic acid; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.01.016