Coeloginin

Base Information

Chemical Name:Coeloginin
CAS No.:82358-34-7
Molecular Formula:C₁₇H₁₄O₆
Molecular Weight:314.295
Hs Code.:
UNII:AT7CHG83PJ
DSSTox Substance ID:DTXSID401031836
Nikkaji Number:J193.268C
Wikidata:Q18348159
Wikipedia:Coeloginin
Mol file:82358-34-7.mol

Synonyms:Coeloginin;AT7CHG83PJ;82358-34-7;UNII-AT7CHG83PJ;9,10-Dihydro-2,6-dihydroxy-7,8-dimethoxy-5H-phenanthro(4,5-bcd)pyran-5-one;9,10-Dihydro-2,6-dihydroxy-7,8-dimethoxy-5H-phenanthro[4,5-bcd]pyran-5-one;5H-Phenanthro(4,5-bcd)pyran-5-one, 9,10-dihydro-2,6-dihydroxy-7,8-dimethoxy-;5H-Phenanthro[4,5-bcd]pyran-5-one, 9,10-dihydro-2,6-dihydroxy-7,8-dimethoxy-;DTXSID401031836

Suppliers and Price of Coeloginin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Coeloginin

Chemical Property:

PSA：89.13000
LogP:2.47320
XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:314.07903816
Heavy Atom Count:23
Complexity:482

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C2C3=C1CCC4=C3C(=CC(=C4)O)OC2=O)O)OC

Technology Process of Coeloginin

There total 27 articles about Coeloginin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1510682-99-1
C₃₂H₂₈O₇

: 82358-34-7
coeloginin

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 72h; under 15001.5 Torr;
DOI:10.1021/ja411146x

Reference yield:

: 6395-18-2
methyl 2,3,4-trimethoxybenzoate

: 82358-34-7
coeloginin

Guidance literature:: Multi-step reaction with 7 steps

1: 4.4 g / hydrogen chloride, zinc chloride / 1,2-dichloro-ethane / 1.) 40 deg C, 3.75 h, 2.) 15 h, RT

2: 1.85 g / toluene / 45 h / 60 °C

3: lithium methoxide / methanol; dimethylformamide

4: 1.034 g / methanol; dimethylformamide / 4.5 h / 90 °C

5: 157 mg / cyclohexane / 4.5 h / Irradiation

6: 214 mg / hydrogen / palladized charcoal / acetic acid / 96 h

7: 22.5 mg / boron trichloride / CH₂Cl₂ / 24 h / Ambient temperature

With hydrogenchloride; lithium methanolate; hydrogen; boron trichloride; zinc(II) chloride; palladium on activated charcoal; In methanol; dichloromethane; cyclohexane; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 94169-66-1
methyl 5-chloromethyl-2,3,4-trimethoxybenzoate

: 82358-34-7
coeloginin

Guidance literature:: Multi-step reaction with 6 steps

1: 1.85 g / toluene / 45 h / 60 °C

2: lithium methoxide / methanol; dimethylformamide

3: 1.034 g / methanol; dimethylformamide / 4.5 h / 90 °C

4: 157 mg / cyclohexane / 4.5 h / Irradiation

5: 214 mg / hydrogen / palladized charcoal / acetic acid / 96 h

6: 22.5 mg / boron trichloride / CH₂Cl₂ / 24 h / Ambient temperature

With lithium methanolate; hydrogen; boron trichloride; palladium on activated charcoal; In methanol; dichloromethane; cyclohexane; acetic acid; N,N-dimethyl-formamide; toluene;