Benzenemethanol, 4-methoxy-a-(1-methylethenyl)-3-(1-methylethoxy)-2-(1-phenyl-1-propen yl)-

Base Information

• Chemical Name: Benzenemethanol, 4-methoxy-a-(1-methylethenyl)-3-(1-methylethoxy)-2-(1-phenyl-1-propen yl)-
• CAS No.: 850404-00-1
• Molecular Formula: C23H28O3
• Molecular Weight: 352.474
• Mol file: 850404-00-1.mol

Synonyms:

Chemical Property of Benzenemethanol, 4-methoxy-a-(1-methylethenyl)-3-(1-methylethoxy)-2-(1-phenyl-1-propen yl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanol, 4-methoxy-a-(1-methylethenyl)-3-(1-methylethoxy)-2-(1-phenyl-1-propen yl)-

There total 1 articles about Benzenemethanol, 4-methoxy-a-(1-methylethenyl)-3-(1-methylethoxy)-2-(1-phenyl-1-propen yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

isopropenylmagnesium bromide (13291-18-4) + 3-isopropoxy-4-methoxy-2-(1-phenyl-1-propenyl)benzaldehyde → 1-[3-isopropoxy-4-methoxy-2-(1-phenyl-1-propenyl)phenyl]-2-methyl-2-propen-1-ol (850404-00-1)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/j.jorganchem.2006.08.074

Reference yield: 82.0%

1-[3-isopropoxy-4-methoxy-2-(1-phenyl-1-propenyl)phenyl]-2-methyl-2-propen-1-ol (850404-00-1) → 4-isopropoxy-5-methoxy-2-methyl-3-phenyl-1H-inden-1-one

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; at 80 ℃; for 16h;

DOI:10.1055/s-2005-862356

Reference yield: 16.0%

1-[3-isopropoxy-4-methoxy-2-(1-phenyl-1-propenyl)phenyl]-2-methyl-2-propen-1-ol (850404-00-1) → 4-isopropoxy-5-methoxy-2-methyl-3-phenyl-1H-inden-1-ol

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In tetrahydrofuran; at 40 ℃; for 8h;

DOI:10.1055/s-2005-862356

upstream raw materials:

isopropenylmagnesium bromide