Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester

Base Information

Chemical Name:Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester
CAS No.:850462-65-6
Molecular Formula:C9H7BrFNO4
Molecular Weight:292.061
Hs Code.:
Mol file:850462-65-6.mol

Synonyms:2-(bromomethyl)-5-fluoro-3-nitrobenzoic acid methylester;

Suppliers and Price of Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemcia Scientific
2-Bromomethyl-5-fluoro-3-nitro-benzoicacidmethylester 95%
5 G
$ 995.00

Total 7 raw suppliers

Chemical Property of Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester

Chemical Property:

PSA：72.12000
LogP:2.93860
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98% ^*data from raw suppliers

2-Bromomethyl-5-fluoro-3-nitro-benzoicacidmethylester 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester

There total 3 articles about Benzoic acid,2-(broMoMethyl)-5-fluoro-3-nitro-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 697739-03-0
5-fluoro-2-methyl-3-nitrobenzoic acid methyl ester

: 850462-65-6
2-bromomethyl-5-fluoro-3-nitrobenzoic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; BPO; In tetrachloromethane; Reflux;

Reference yield: 75.9%

: 697739-03-0
5-fluoro-2-methyl-3-nitrobenzoic acid methyl ester

: 123-56-8,89963-74-6
Succinimide

: 850462-65-6
2-bromomethyl-5-fluoro-3-nitrobenzoic acid methyl ester

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 96h; Heating / reflux;

Reference yield:

: 33184-16-6
5-fluoro-2-methylbenzoic acid

: 850462-65-6
2-bromomethyl-5-fluoro-3-nitrobenzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: nitric acid / sulfuric acid / 3.5 h / -5 - 0 °C

2: thionyl chloride / methanol / 16 h / 0 °C / Reflux

3: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / Reflux

With N-Bromosuccinimide; thionyl chloride; nitric acid; dibenzoyl peroxide; sulfuric acid; In methanol; tetrachloromethane;