Technology Process of Gold, [(4-amino-3-methylphenyl)ethynyl]-
There total 1 articles about Gold, [(4-amino-3-methylphenyl)ethynyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
dichloromethane;
to soln. 2-methyl-4-ethynylaniline in CH2Cl2 Et3N and (AuCl(SMe2)) were added successively and stirred for 1 h; soln. was concd. in vacuo, MeOH was added, ppt. was filtered, washed with Et2O and air-dried; elem. anal.;
DOI:10.1016/j.ica.2004.06.068
- Guidance literature:
-
In
dichloromethane;
to suspn. Au complex in CH2Cl2 XylNC was added and stirred for 0.5 h; soln. was filtered and concd. in vacuo, Et2O was added and stirred for 15 min, ppt. was filtered and air-dried; elem. anal.;
DOI:10.1016/j.ica.2004.06.068
- Guidance literature:
-
In
dichloromethane;
to suspn. Au complex in CH2Cl2 P(C6H4OMe-4)3 was added and stirred for 1h; soln. was filtered and concd. in vacuo, mixt. Et2O and hexane was added and stirred for 15 min, ppt. was filtered and air-dried; elem. anal.;
DOI:10.1016/j.ica.2004.06.068
