2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide

Base Information

Chemical Name:2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide
CAS No.:66066-58-8
Molecular Formula:C13H11NO2S
Molecular Weight:245.2969
Hs Code.:
DSSTox Substance ID:DTXSID90984562

Synonyms:2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide;5-Oxo-7-phenyl-2,3,5-trihydrothiazolo(3,2-a)pyridine-1-oxide;5H-Thiazolo(3,2-a)pyridin-5-one, 2,3-dihydro-7-phenyl-, 1-oxide;66066-58-8;SCHEMBL11363537;DTXSID90984562;LS-152091;7-Phenyl-2,3-dihydro-1lambda~4~-[1,3]thiazolo[3,2-a]pyridine-1,5-dione

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide

Chemical Property:

Vapor Pressure:1.17E-13mmHg at 25°C
Boiling Point:584.8°Cat760mmHg
Flash Point:307.5°C
Density:1.46g/cm³
XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:245.05104977
Heavy Atom Count:17
Complexity:433

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CS(=O)C2=CC(=CC(=O)N21)C3=CC=CC=C3

Technology Process of 2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide

There total 5 articles about 2,3-Dihydro-7-phenyl-5H-thiazolo(3,2-a)pyridin-5-one 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66066-14-6
7-phenyl-2,3-dihydro-thiazolo[3,2-a]pyridin-5-one

: 66066-58-8
1-oxo-7-phenyl-2,3-dihydro-1H-1λ⁴-thiazolo[3,2-a]pyridin-5-one

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 15h; Ambient temperature;
DOI:10.1248/cpb.27.1207

Reference yield:

: 25297-57-8
6-chloro-1-methyl-4-phenyl-1H-pyridin-2-one

: 66066-58-8
1-oxo-7-phenyl-2,3-dihydro-1H-1λ⁴-thiazolo[3,2-a]pyridin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: ethane-1,2-diol / 190 - 200 °C

2: aq. H₂O₂ / acetic acid / 15 h / Ambient temperature

With dihydrogen peroxide; In ethylene glycol; acetic acid;
DOI:10.1248/cpb.27.1207

Reference yield:

: 71858-44-1
6-(2-amino-ethylsulfanyl)-1-(4-chloro-phenyl)-4-phenyl-pyridin-2-one; hydrochloride

: 66066-58-8
1-oxo-7-phenyl-2,3-dihydro-1H-1λ⁴-thiazolo[3,2-a]pyridin-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: ethane-1,2-diol / 3 h / 190 - 200 °C

2: aq. H₂O₂ / acetic acid / 15 h / Ambient temperature

With dihydrogen peroxide; In ethylene glycol; acetic acid;
DOI:10.1248/cpb.27.1207