Perithiaden

Base Information

Chemical Name:Perithiaden
CAS No.:1447-70-7
Molecular Formula:C₂₀H₂₁NS
Molecular Weight:307.459
Hs Code.:
DSSTox Substance ID:DTXSID90932386

Synonyms:Perithiaden;1447-70-7;4-(6H-benzo[c][1]benzothiepin-11-ylidene)-1-methylpiperidine;4-(dibenzo[b,e]thiepin-11(6h)-ylidene)-1-methylpiperidine;SCHEMBL7297067;DTXSID90932386;MBGXTYVKSKOCFX-UHFFFAOYSA-N;4-(Dibenzo(b,e)thiepin-6(11H)-ylidene)-1-methylpiperidine hydrochlorine;Piperidine, 4-(dibenzo(b,e)thiepin-6(11H)-ylidene)-1-methyl-, hydrochloride;AE-641/30103008;4-dibenzo[b,e]thiepin-11(6H)-ylidene-1-methylpiperidine;4-(6,11-dihydrodibenzo[b,e]thiepin-11-ylidene)-1-methylpiperidine

Suppliers and Price of Perithiaden

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Perithiaden

Chemical Property:

Vapor Pressure:7.75E-09mmHg at 25°C
Boiling Point:465.3°Cat760mmHg
Flash Point:235.2°C
Density:1.165g/cm³
XLogP3:4.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:307.13947085
Heavy Atom Count:22
Complexity:419

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1CCC(=C2C3=CC=CC=C3CSC4=CC=CC=C42)CC1

Technology Process of Perithiaden

There total 5 articles about Perithiaden which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1531-82-4
11-(1-methyl-4-piperidyl)-6,11-dihydrodibenzothiepin-11-ol

: 1447-70-7
11-(1-methyl-4-piperidylidene)-6,11-dihydrodibenzothiepin

Guidance literature:: With hydrogenchloride; In acetic acid; for 1h; Heating;
DOI:10.1002/hlca.19620450616

Reference yield:

: 5570-77-4
4-chloro-1-methylpiperidine

: 1447-70-7
11-(1-methyl-4-piperidylidene)-6,11-dihydrodibenzothiepin

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, BrCH₂CH₂Br, I₂, THF, (ii) /BRN= 782673/

2: aq. HCl / acetic acid / 1 h / Heating

With hydrogenchloride; In acetic acid;
DOI:10.1002/hlca.19620450616

Reference yield:

: 1531-77-7
dibenzo[b,e]thiepin-11(6H)-one

: 1447-70-7
11-(1-methyl-4-piperidylidene)-6,11-dihydrodibenzothiepin

Guidance literature:: Multi-step reaction with 2 steps

1: (i) Mg, BrCH₂CH₂Br, I₂, THF, (ii) /BRN= 782673/

2: aq. HCl / acetic acid / 1 h / Heating

With hydrogenchloride; In acetic acid;
DOI:10.1002/hlca.19620450616