Arthothelin

Base Information

Chemical Name:Arthothelin
CAS No.:20716-96-5
Molecular Formula:C14H7Cl3O5
Molecular Weight:361.5614
Hs Code.:2932999099
NSC Number:295145
DSSTox Substance ID:DTXSID60174776
Nikkaji Number:J16.803C
Wikidata:Q83044914
Mol file:20716-96-5.mol

Synonyms:ARTHOTHELIN;20716-96-5;2,4,5-trichloro-1,3,6-trihydroxy-8-methylxanthen-9-one;9H-Xanthen-9-one, 2,4,5-trichloro-1,3,6- trihydroxy-8-methyl-;Xanthen-9-one, 2,4,7-trichloro-1,3,6-trihydroxy-8-methyl-;9H-Xanthen-9-one, 2,4,5-trichloro-1,3,6-trihydroxy-8-methyl-;NSC295145;2,4,5-trichloronorlichexanthone;DTXSID60174776;CHEBI:144075;NTAXLEHKEDVPRK-UHFFFAOYSA-N;NSC 295145;NSC-295145;Xanthen-9-one,4,7-trichloro-1,3,6-trihydroxy-8-methyl-;2,4,5-Trichloro-1,3,6-trihydroxy-8-methyl-9H-xanthen-9-one;9H-Xanthen-9-one,4,5-trichloro-1,3,6-trihydroxy-8-methyl-;Xanthen-9-one, 2,4,5-trichloro-1,3,6-trihydroxy-8-methyl-;2,4,5-Trichloro-1,3,6-trihydroxy-8-methyl-9H-xanthen-9-one #;9H-Xanthen-9-one, 2,4,7-trichloro-1,3,6-trihydroxy-8-methyl-

Suppliers and Price of Arthothelin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Arthothelin

Chemical Property:

Vapor Pressure:1.43E-13mmHg at 25°C
Boiling Point:569.5°Cat760mmHg
Flash Point:298.2°C
PSA：90.90000
Density:1.798g/cm³
LogP:4.33160
XLogP3:4.7
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:0
Exact Mass:359.935906
Heavy Atom Count:22
Complexity:464

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C2=C1C(=O)C3=C(C(=C(C(=C3O2)Cl)O)Cl)O)Cl)O

Technology Process of Arthothelin

There total 12 articles about Arthothelin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 20716-96-5
arthothelin

Guidance literature:: Multi-step reaction with 7 steps

1: 2.7 g / trifluoroacetic anhydride / CH₂Cl₂ / 0.17 h / 0 °C

2: hydrogen, aq. hydrochloric acid / palladized charcoal / ethyl acetate

3: 850 mg / potassium hydroxide / ethanol / 1.5 h / Heating

4: pyridine / 90 °C

5: 3.0 g / sulphuryl chloride / CH₂Cl₂

6: boron trichloride / CH₂Cl₂ / 1 h / 0 °C

7: 385 mg / piperidine, water / 3 h / Heating

With piperidine; pyridine; hydrogenchloride; potassium hydroxide; sulfuryl dichloride; water; hydrogen; boron trichloride; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;

Reference yield:

: 38103-07-0
methyl 3-chloro-2,4-dihydroxy-6-methylbenzoate

: 20716-96-5
arthothelin

Guidance literature:: Multi-step reaction with 9 steps

1: 10.4 g / potassium carbonate / dimethylformamide / 15 h

2: 9.7 g / potassium hydroxide, water / dimethylsulfoxide / 6 h / Heating

3: 2.7 g / trifluoroacetic anhydride / CH₂Cl₂ / 0.17 h / 0 °C

4: hydrogen, aq. hydrochloric acid / palladized charcoal / ethyl acetate

5: 850 mg / potassium hydroxide / ethanol / 1.5 h / Heating

6: pyridine / 90 °C

7: 3.0 g / sulphuryl chloride / CH₂Cl₂

8: boron trichloride / CH₂Cl₂ / 1 h / 0 °C

9: 385 mg / piperidine, water / 3 h / Heating

With piperidine; pyridine; hydrogenchloride; potassium hydroxide; sulfuryl dichloride; water; hydrogen; boron trichloride; potassium carbonate; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 72911-57-0
methyl 2,4-bisbenzyloxy-3-chloro-6-methylbenzoate

: 20716-96-5
arthothelin

Guidance literature:: Multi-step reaction with 8 steps

1: 9.7 g / potassium hydroxide, water / dimethylsulfoxide / 6 h / Heating

2: 2.7 g / trifluoroacetic anhydride / CH₂Cl₂ / 0.17 h / 0 °C

3: hydrogen, aq. hydrochloric acid / palladized charcoal / ethyl acetate

4: 850 mg / potassium hydroxide / ethanol / 1.5 h / Heating

5: pyridine / 90 °C

6: 3.0 g / sulphuryl chloride / CH₂Cl₂

7: boron trichloride / CH₂Cl₂ / 1 h / 0 °C

8: 385 mg / piperidine, water / 3 h / Heating

With piperidine; pyridine; hydrogenchloride; potassium hydroxide; sulfuryl dichloride; water; hydrogen; boron trichloride; trifluoroacetic anhydride; palladium on activated charcoal; In ethanol; dichloromethane; dimethyl sulfoxide; ethyl acetate;