1H-Pyrrol-1-yloxy, 3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl-

Base Information

Chemical Name:1H-Pyrrol-1-yloxy, 3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl-
CAS No.:851025-48-4
Molecular Formula:C₂₉H₃₃I₂N₂O₄
Molecular Weight:727.401
Hs Code.:

1H-Pyrrol-1-yloxy,
3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth
ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl-

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Chemical Property of 1H-Pyrrol-1-yloxy, 3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl-

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Technology Process of 1H-Pyrrol-1-yloxy, 3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl-

There total 3 articles about 1H-Pyrrol-1-yloxy, 3-[[[2-[2,6-diiodo-4-[(2-methyl-3-benzofuranyl)carbonyl]phenoxy]ethyl]eth ylamino]methyl]-2,5-dihydro-2,2,5,5-tetramethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 851025-42-8
C₁₄H₂₇N₂O₄S

: 10402-56-9
2-methyl-3-(3,5-diiodo-4-hydroxybenzoyl)benzofuran

: 851025-48-4
2-methyl-3-(3,5-diiodo-4-{2-[N-ethyl,N-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)amino]ethyl}oxybenzoyl)benzofuran

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In acetone; for 24h; Heating;
DOI:10.1016/j.bmc.2005.01.028

Reference yield:

: 851025-44-0
3-{[ethyl-(2-hydroxyethyl)-amino]-methyl}-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-1-yloxyl

: 851025-48-4
2-methyl-3-(3,5-diiodo-4-{2-[N-ethyl,N-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)amino]ethyl}oxybenzoyl)benzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / triethylamine / CH₂Cl₂ / 1 h / 0 - 20 °C

2: 58 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

With 18-crown-6 ether; potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.1016/j.bmc.2005.01.028

Reference yield:

: 76893-32-8
3-(bromomethyl)-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-oxyl

: 851025-48-4
2-methyl-3-(3,5-diiodo-4-{2-[N-ethyl,N-(1-oxyl-2,2,5,5-tetramethyl-2,5-dihydro-1H-pyrrol-3-ylmethyl)amino]ethyl}oxybenzoyl)benzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / K₂CO₃ / CHCl₃ / 4 h / Heating

2: 66 percent / triethylamine / CH₂Cl₂ / 1 h / 0 - 20 °C

3: 58 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

With 18-crown-6 ether; potassium carbonate; triethylamine; In dichloromethane; chloroform; acetone;
DOI:10.1016/j.bmc.2005.01.028