Cobalt(3+), bis(N-(2-aminoethyl)-1,2-ethanediamine-N,N',N'')-

Base Information

• Chemical Name: Cobalt(3+), bis(N-(2-aminoethyl)-1,2-ethanediamine-N,N',N'')-
• CAS No.: 18703-28-1
• Molecular Formula: C₈H₂₆CoN₆
• Molecular Weight: 265.328
• DSSTox Substance ID: DTXSID60171967
• Mol file: 18703-28-1.mol

Synonyms:Co(trien) complex;cobalt triethylene tetramine complex

Chemical Property of Cobalt(3+), bis(N-(2-aminoethyl)-1,2-ethanediamine-N,N',N'')-

Chemical Property:

• Vapor Pressure: 0.232mmHg at 25°C
• Boiling Point: 206.9°Cat760mmHg
• Flash Point: 94.4°C
• PSA: 128.14000
• Density: g/cm³
• LogP: 0.56980
• Hydrogen Bond Donor Count: 6
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 8
• Exact Mass: 265.155088
• Heavy Atom Count: 15
• Complexity: 26.1

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CNCCN)N.C(CNCCN)N.[Co+3]

Technology Process of Cobalt(3+), bis(N-(2-aminoethyl)-1,2-ethanediamine-N,N',N'')-

There total 11 articles about Cobalt(3+), bis(N-(2-aminoethyl)-1,2-ethanediamine-N,N',N'')- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[Co(N-(2-aminoethyl)ethane-1,2-diamine)2](2+) (23624-01-3,67145-48-6,67145-47-5,67145-46-4) → Co(HN(C2H4NH2)2)2(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + C8H26CoN6(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + [Co(dien)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + Δ-fac-[Co((NH2CH2CH2)2NH)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6)

Guidance literature:

With lithium chloride; In formamide; Co(III) oxidant was added to Co(II) complex generated in situ in formamide in the presence of LiCl (ionic strength of 0.12-0.18 M) at 25°; after a complete disappearance of oxidant color (5-45 min), the reaction was quenched with 3 M HCl; separation of geometrical isomers on SP-Sephadex column; detected by UVand CD spectra;

DOI:10.1246/bcsj.73.1135

Reference yield:

[Co(N-(2-aminoethyl)ethane-1,2-diamine)2](2+) (23624-01-3,67145-48-6,67145-47-5,67145-46-4) → Co(HN(C2H4NH2)2)2(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + C8H26CoN6(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + [Co(dien)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + Δ-fac-[Co((NH2CH2CH2)2NH)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6)

Guidance literature:

With lithium chloride; In formamide; Co(III) oxidant was added to Co(II) complex generated in situ in formamide in the presence of LiCl (ionic strength of 0.12-0.18 M) at 25°; after a complete disappearance of oxidant color (5-45 min), the reaction was quenched with 3 M HCl; separation of geometrical isomers on SP-Sephadex column; detected by UVand CD spectra;

DOI:10.1246/bcsj.73.1135

Reference yield:

[Co(N-(2-aminoethyl)ethane-1,2-diamine)2](2+) (23624-01-3,67145-48-6,67145-47-5,67145-46-4) → Co(HN(C2H4NH2)2)2(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + C8H26CoN6(3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + [Co(dien)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6) + Δ-fac-[Co((NH2CH2CH2)2NH)2](3+) (110693-79-3,18703-28-1,29530-89-0,29636-13-3,29636-14-4,38318-04-6,38318-05-7,38318-06-8,48145-49-9,778525-21-6)

Guidance literature:

With lithium chloride; In formamide; Co(III) oxidant was added to Co(II) complex generated in situ in formamide in the presence of LiCl (ionic strength of 0.12-0.18 M) at 25°; after a complete disappearance of oxidant color (5-45 min), the reaction was quenched with 3 M HCl; separation of geometrical isomers on SP-Sephadex column; detected by UVand CD spectra;

DOI:10.1246/bcsj.73.1135

upstream raw materials:

[Co(N-(2-aminoethyl)ethane-1,2-diamine)2]⁽²⁺⁾

(3-azapentane-1,5-diamine)trichlorocobalt(III)

mer-trichloro(N-(3-aminopropyl)-1,3-diaminopropane)cobalt(III)

mer-{(3-azapentane-1,5-diamine)trichlorocobalt(III)}

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