N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Base Information

Chemical Name:N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide
CAS No.:10019-03-1
Molecular Formula:C17H13 N2 O7 P
Molecular Weight:388.273
Hs Code.:2924299090
European Community (EC) Number:233-014-2
DSSTox Substance ID:DTXSID40142998
Nikkaji Number:J241.219E
Wikidata:Q83006635
Mol file:10019-03-1.mol

Synonyms:10019-03-1;NAPHTHOL AS-BS PHOSPHATE;N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide;Naphthol as-bs-phosphate;EINECS 233-014-2;[3-[(3-nitrophenyl)carbamoyl]naphthalen-2-yl] dihydrogen phosphate;SCHEMBL11979381;C17H13N2O7P;DTXSID40142998;C17-H13-N2-O7-P;STL301823;AKOS015913299;FT-0752103;N-(3-Nitrophenyl)-3-(phosphonooxy)-2-naphthalenecarboxamide;3-[(3-nitrophenyl)carbamoyl]naphthalen-2-yl dihydrogen phosphate

Suppliers and Price of N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
NAPHTHOL AS-BS PHOSPHATE 95.00%
5G
$ 1388.60

Total 9 raw suppliers

Chemical Property of N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Chemical Property:

Boiling Point:°Cat760mmHg
PKA:1.03±0.30(Predicted)
Flash Point:°C
PSA：151.49000
Density:1.611g/cm³
LogP:4.06800
Storage Temp.:2-8°C
XLogP3:2.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:388.04603776
Heavy Atom Count:27
Complexity:605

Purity/Quality:

98%,99%, ^*data from raw suppliers

NAPHTHOL AS-BS PHOSPHATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:C1=CC=C2C=C(C(=CC2=C1)C(=O)NC3=CC(=CC=C3)[N+](=O)[O-])OP(=O)(O)O

Technology Process of N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

There total 4 articles about N-(3-Nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 135-65-9
3-hydroxy-3'-nitro-2-naphthanilide

: 10019-03-1
N-(3-nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Guidance literature:: With phosphorus pentachloride; In 1,4-dioxane; at 50 ℃; for 1h;
DOI:10.1021/ac00080a022

Reference yield:

: 10019-03-1
N-(3-nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Guidance literature:: 2-Hydroxy-naphthalin-3-carbonsaeure-<3-nitro-anilid> 1) in Dioxan u. POCl3 u. Py. 2) + W.;

Reference yield:

: 99-09-2
3-nitro-aniline

: 10019-03-1
N-(3-nitrophenyl)-3-(phosphonooxy)naphthalene-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) PCl₃ / 1) xylene, 80 deg C, 10 min; 2) xylene, reflux, 2 h

2: PCl₅ / dioxane / 1 h / 50 °C

With phosphorus pentachloride; phosphorus trichloride; In 1,4-dioxane;
DOI:10.1021/ac00080a022