Hydroxylamine, O-[(2,4-difluorophenyl)methyl]-

Base Information

Chemical Name:Hydroxylamine, O-[(2,4-difluorophenyl)methyl]-
CAS No.:851180-94-4
Molecular Formula:C7H7F2NO
Molecular Weight:159.135
Hs Code.:

Synonyms:

Suppliers and Price of Hydroxylamine, O-[(2,4-difluorophenyl)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Hydroxylamine, O-[(2,4-difluorophenyl)methyl]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Hydroxylamine, O-[(2,4-difluorophenyl)methyl]-

There total 3 articles about Hydroxylamine, O-[(2,4-difluorophenyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₉F₂NO₃

: 851180-94-4
O-(2,4-difluorobenzyl)hydroxylamine

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2015.12.028

Reference yield:

: 56456-47-4
2,4-difluorobenzyl alcohol

: 851180-94-4
O-(2,4-difluorobenzyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: hydrazine hydrate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; 1: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2015.12.028

Reference yield:

: 1550-35-2
2,4-difluorobenzaldehyde

: 851180-94-4
O-(2,4-difluorobenzyl)hydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 0 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

3: hydrazine hydrate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; methanol; 2: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2015.12.028