Silane, [[(3R)-3-azidodecyl]oxy](1,1-dimethylethyl)diphenyl-

Base Information

Chemical Name:Silane, [[(3R)-3-azidodecyl]oxy](1,1-dimethylethyl)diphenyl-
CAS No.:851303-98-5
Molecular Formula:C26H39N3OSi
Molecular Weight:437.701
Hs Code.:

Synonyms:

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Chemical Property of Silane, [[(3R)-3-azidodecyl]oxy](1,1-dimethylethyl)diphenyl-

Chemical Property:

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Safty Information:

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Technology Process of Silane, [[(3R)-3-azidodecyl]oxy](1,1-dimethylethyl)diphenyl-

There total 6 articles about Silane, [[(3R)-3-azidodecyl]oxy](1,1-dimethylethyl)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 851303-96-3
C₂₇H₄₂O₄SSi

: 851303-98-5
C₂₆H₃₉N₃OSi

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 140 ℃;
DOI:10.1016/j.bmcl.2005.08.080

Reference yield:

: 128387-27-9
(R)-decane-1,3-diol

: 851303-98-5
C₂₆H₃₉N₃OSi

Guidance literature:: Multi-step reaction with 5 steps

1: dmap; triethylamine / dichloromethane / 20 h / 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / -20 - 0 °C

3: potassium carbonate / tetrahydrofuran; methanol / 4 h / 20 °C

4: dmap; triethylamine / dichloromethane / 0 - 20 °C

5: sodium azide / N,N-dimethyl-formamide / 140 °C

With dmap; sodium azide; potassium carbonate; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 581782-27-6
C₂₆H₄₀O₂Si

: 851303-98-5
C₂₆H₃₉N₃OSi

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / -20 - 0 °C

2: potassium carbonate / tetrahydrofuran; methanol / 4 h / 20 °C

3: dmap; triethylamine / dichloromethane / 0 - 20 °C

4: sodium azide / N,N-dimethyl-formamide / 140 °C

With dmap; sodium azide; potassium carbonate; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;