Cycloheptanecarboxamide, N-methyl-N-phenyl-

Base Information

Chemical Name:Cycloheptanecarboxamide, N-methyl-N-phenyl-
CAS No.:851980-78-4
Molecular Formula:C15H21NO
Molecular Weight:231.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cycloheptanecarboxamide, N-methyl-N-phenyl-

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Technology Process of Cycloheptanecarboxamide, N-methyl-N-phenyl-

There total 1 articles about Cycloheptanecarboxamide, N-methyl-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 6557-86-4
cycloheptanecarbonyl chloride

: 100-61-8
N-methylaniline

: 851980-78-4
cycloheptanecarboxylic acid methyl-phenyl-amide

Guidance literature:: With triethylamine; In 1,4-dioxane; for 2h; Heating;
DOI:10.1002/hlca.200490216

Reference yield: 79.0%

: 851980-78-4
cycloheptanecarboxylic acid methyl-phenyl-amide

: 803738-94-5
(1-aza-spiro[2.6]non-1-en-2-yl)-methyl-phenyl-amine

Guidance literature:: cycloheptanecarboxylic acid methyl-phenyl-amide; With n-butyllithium; diisopropylamine; In tetrahydrofuran; pentane; at 0 ℃; for 1h;

With chlorophosphoric acid diphenyl ester; In tetrahydrofuran; pentane; at 0 - 20 ℃; for 24.5h;

With sodium azide; In N,N-dimethyl-formamide; at 20 ℃; for 96h;
DOI:10.1002/hlca.200490216

Reference yield:

: 851980-78-4
cycloheptanecarboxylic acid methyl-phenyl-amide

: 803739-25-5
1',3'-dihydro-1'-methylspiro[cycloheptane-1,3'-[2H]indol]-2'-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: (i-Pr)2NH; BuLi / tetrahydrofuran; pentane / 1 h / 0 °C

1.2: diphenyl phosphorochloridate / tetrahydrofuran; pentane / 24.5 h / 0 - 20 °C

1.3: 79 percent / NaN₃ / dimethylformamide / 96 h / 20 °C

2.1: 60 percent / BF₃*OEt₂ / tetrahydrofuran / 12 h / 23 °C

3.1: 31 percent / pyridine / 16 h / 23 °C

With n-butyllithium; boron trifluoride diethyl etherate; diisopropylamine; In tetrahydrofuran; pyridine; pentane;
DOI:10.1002/hlca.200490216