Propanedioic acid, dodecyl[[2-[(phenylmethyl)seleno]-3-pyridinyl]methyl]-, monoethyl ester

Base Information

Chemical Name:Propanedioic acid, dodecyl[[2-[(phenylmethyl)seleno]-3-pyridinyl]methyl]-, monoethyl ester
CAS No.:852063-28-6
Molecular Formula:C30H43NO4Se
Molecular Weight:560.636
Hs Code.:

Synonyms:

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Chemical Property of Propanedioic acid, dodecyl[[2-[(phenylmethyl)seleno]-3-pyridinyl]methyl]-, monoethyl ester

Chemical Property:

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Technology Process of Propanedioic acid, dodecyl[[2-[(phenylmethyl)seleno]-3-pyridinyl]methyl]-, monoethyl ester

There total 8 articles about Propanedioic acid, dodecyl[[2-[(phenylmethyl)seleno]-3-pyridinyl]methyl]-, monoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 852063-27-5
tert-butyl ethyl 2-[2-(benzylseleno)pyridin-3-ylmethyl]-2-dodecylmalonate

: 852063-28-6
2-(ethoxycarbonyl)-2-[2-(benzylseleno)pyridin-3-ylmethyl]tetradecanoic acid

Guidance literature:: With trifluoroacetic acid;
DOI:10.3390/90600472

Reference yield:

: 32864-38-3
tert-Butyl ethyl malonate

: 852063-28-6
2-(ethoxycarbonyl)-2-[2-(benzylseleno)pyridin-3-ylmethyl]tetradecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / various solvent(s); tetrahydrofuran / 0.5 h / 20 °C

1.2: 54 percent / various solvent(s); tetrahydrofuran / 18 h / Heating

2.1: sodium hydride / various solvent(s); tetrahydrofuran / 0.5 h / 0 °C

2.2: 74 percent / various solvent(s); tetrahydrofuran / 5 h / Heating

3.1: 67 percent / trifluoroacetic acid / CH₂Cl₂ / 1 h / 0 °C

With sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b515385a

Reference yield:

: 1482-82-2
dibenzyl diselenide

: 852063-28-6
2-(ethoxycarbonyl)-2-[2-(benzylseleno)pyridin-3-ylmethyl]tetradecanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium borohydride / ethanol

1.2: 71 percent / ethanol / 3 h / Heating

2.1: 97 percent / LiAlH₄ / diethyl ether / 1.5 h / 20 °C

3.1: 96 percent / triethylamine; methanesulfonyl chloride / tetrahydrofuran / 1 h / Heating

4.1: sodium hydride / various solvent(s); tetrahydrofuran / 0.5 h / 20 °C

4.2: 54 percent / various solvent(s); tetrahydrofuran / 18 h / Heating

5.1: sodium hydride / various solvent(s); tetrahydrofuran / 0.5 h / 0 °C

5.2: 74 percent / various solvent(s); tetrahydrofuran / 5 h / Heating

6.1: 67 percent / trifluoroacetic acid / CH₂Cl₂ / 1 h / 0 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; sodium hydride; methanesulfonyl chloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1039/b515385a