1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester

Base Information

Chemical Name:1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester
CAS No.:859857-53-7
Molecular Formula:C13H12O5
Molecular Weight:248.235
Hs Code.:

Synonyms:dimethyl-5-(prop-2-ynyloxy)isophthalic acid;dimethyl 5-(prop-2-ynyloxy)isophthalate;dimethyl 5-propargyloxyisophthalate;1,3-Benzenedicarboxylic acid,5-(2-propynyloxy)-,dimethyl ester;dimethyl 5-hydroxyisophtalate propargyl ether;dimethyl 5-hydroxyisophthalate propargyl ether;propargyl ether of dimethyl 5-hydroxyisophthalate;

Suppliers and Price of 1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester

Chemical Property:

PSA：61.83000
LogP:1.27180

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester

There total 2 articles about 1,3-Benzenedicarboxylic acid, 5-(2-propynyloxy)-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 106-96-7
propargyl bromide

: 859857-53-7
5-(prop-2-ynyloxy)isophthalic acid dimethyl ester

Guidance literature:: Dimethyl 5-hydroxyisophthalate; With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 1h;

propargyl bromide; In N,N-dimethyl-formamide; at 20 - 25 ℃;

Reference yield:

: 618-83-7
5-Hydroxyisophthalic acid

: 859857-53-7
5-(prop-2-ynyloxy)isophthalic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: potassium carbonate / acetone / Reflux

With sulfuric acid; potassium carbonate; In acetone;
DOI:10.1039/c6dt00658b