Benzoic acid, 2,4,6-trinitro-, 2,2,2-trinitroethyl ester

Base Information

• Chemical Name: Benzoic acid, 2,4,6-trinitro-, 2,2,2-trinitroethyl ester
• CAS No.: 860-83-3
• Molecular Formula: C9H4N6O14
• Molecular Weight: 420.163
• Mol file: 860-83-3.mol

Synonyms:

Chemical Property of Benzoic acid, 2,4,6-trinitro-, 2,2,2-trinitroethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2,4,6-trinitro-, 2,2,2-trinitroethyl ester

There total 4 articles about Benzoic acid, 2,4,6-trinitro-, 2,2,2-trinitroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2,2,2-trinitroethanol (918-54-7) + 2,4,6-trinitrobenzoic acid (129-66-8) → 2,2,2-trinitroethyl 2,4,6-trinitrobenzoate (860-83-3)

Guidance literature:

2,2,2-trinitroethanol; With chlorosulfonic acid; at -10 - 50 ℃; for 1h;

2,4,6-trinitrobenzoic acid; at 80 ℃; for 2h; Temperature;

DOI:10.1039/C6NJ02198K

Reference yield: 80.0%

2,4,6-trinitrobenzoic acid (129-66-8) + 2,2,2-Trinitroethyl hydrogen sulfate (66881-27-4) → 2,2,2-trinitroethyl 2,4,6-trinitrobenzoate (860-83-3)

Guidance literature:

at 100 ℃; for 3h;

Reference yield:

2,4,6-Trinitrotoluene (118-96-7) → 2,2,2-trinitroethyl 2,4,6-trinitrobenzoate (860-83-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium dichromate; sulfuric acid

2.1: chlorosulfonic acid / 1 h / -10 - 50 °C

2.2: 2 h / 80 °C

With chlorosulfonic acid; potassium dichromate; sulfuric acid;

DOI:10.1039/C6NJ02198K

upstream raw materials:

2,4,6-trinitrobenzoic acid

2,2,2-Trinitroethyl hydrogen sulfate

2,2,2-trinitroethanol

2,4,6-Trinitrotoluene