1-(1-Cyclohexenyl)-3-ethoxy-2-propanone

Base Information

• Chemical Name: 1-(1-Cyclohexenyl)-3-ethoxy-2-propanone
• CAS No.: 51149-72-5
• Molecular Formula: C₁₁H₁₈O₂
• Molecular Weight: 182.263
• Hs Code.: 2914509090
• Mol file: 51149-72-5.mol

Synonyms:2-Propanone,1-(1-cyclohexen-1-yl)-3-ethoxy;1-cyclohexenyl-3-ethoxy-2-propanone;1-(1-Cyclohexen-1-yl)-3-ethoxyacetone;

Chemical Property of 1-(1-Cyclohexenyl)-3-ethoxy-2-propanone

Chemical Property:

• Vapor Pressure: 0.00472mmHg at 25°C
• Boiling Point: 276.7°Cat760mmHg
• Flash Point: 112.3°C
• PSA: 26.30000
• Density: 0.967g/cm³
• LogP: 2.48250

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(1-Cyclohexenyl)-3-ethoxy-2-propanone

There total 2 articles about 1-(1-Cyclohexenyl)-3-ethoxy-2-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Cyclohexen-(1)-yl-propin-(2)-al-(1)-diethylacetal (18229-79-3) → 1-cyclohexenyl-3-ethoxy-2-propanone (51149-72-5)

Guidance literature:

Multistep reaction; (i) disiamylborane, THF, (ii) aq. NaOH, aq. H₂O₂;

DOI:10.1021/ja00808a084

Reference yield:

1-(1'-diazo-2'-oxoprop-3'-yl)cyclohexene (54495-73-7) → 1,4,5,6,7,7a-hexahydro-inden-2-one (39163-29-6,117780-10-6) + 1-cyclohexenyl-3-ethoxy-2-propanone (51149-72-5)

Guidance literature:

copper(II) bis(trifluoromethanesulfonate); In diethyl ether; Product distribution;

DOI:10.1021/jo00181a010

upstream raw materials:

3-Cyclohexen-⁽¹⁾-yl-propin-⁽²⁾-al-⁽¹⁾-diethylacetal

1-(1'-diazo-2'-oxoprop-3'-yl)cyclohexene

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