2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one

Base Information

Chemical Name:2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one
CAS No.:86421-71-8
Molecular Formula:C6H8N2O
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID90522160
Nikkaji Number:J854.412C

Synonyms:2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one;86421-71-8;DTXSID90522160

Suppliers and Price of 2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one

Chemical Property:

XLogP3:-0.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:124.063662883
Heavy Atom Count:9
Complexity:209

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=NC2C1C(=O)N2C

Technology Process of 2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one

There total 2 articles about 2,5-Dimethyl-2,6-diazabicyclo[2.2.0]hex-5-en-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17758-19-9
3,6-dimethylpyrimidin-4(3H)-one

: 86421-71-8
3,6-dimethyl-2,6-diazabicyclo<2.2.0>hex-2-en-5-one

Guidance literature:: In methanol; at -40 - -10 ℃; for 11h; Irradiation;
DOI:10.1021/jo00165a025

Reference yield:

: 86421-86-5
(E)-3-(Dimethoxymethyl-amino)-but-2-enoic acid methylamide

: 86421-71-8
3,6-dimethyl-2,6-diazabicyclo<2.2.0>hex-2-en-5-one

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / H₂O / 0.5 h / 20 - 25 °C

2: 30 percent Spectr_. / methanol / 11 h / -40 - -10 °C / Irradiation

In methanol; water;
DOI:10.1021/jo00165a025