3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)-

Base Information

Chemical Name:3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)-
CAS No.:864448-31-7
Molecular Formula:C20H25N3
Molecular Weight:307.439
Hs Code.:
Mol file:864448-31-7.mol

Synonyms:3,7,9-Triazabicyclo[3.3.1]nonane,3,9-bis(phenylmethyl);

Suppliers and Price of 3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Synthonix
3,7,9-Triazabicyclo[3.3.1]nonane,3,9-bis(phenylmethyl)- 95+%
1g
$ 2270.00

Matrix Scientific
3,7,9-Triazabicyclo[3.3.1]nonane
1g
$ 3994.00

Crysdot
3,7,9-Triazabicyclo[3.3.1]nonane 95+%
100mg
$ 435.00

Chemenu
3,7,9-Triazabicyclo[3.3.1]nonane 95%
100mg
$ 410.00

Total 6 raw suppliers

Chemical Property of 3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)-

Chemical Property:

PSA：18.51000
LogP:2.54940

Purity/Quality:

97% ^*data from raw suppliers

3,7,9-Triazabicyclo[3.3.1]nonane,3,9-bis(phenylmethyl)- 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 3,9-Dibenzyl-3,7,9-triazabicyclo[3.3.1]nonane is an intermediate used in the preparation of piperazine based building blocks.

Technology Process of 3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)-

There total 1 articles about 3,7,9-Triazabicyclo[3.3.1]nonane, 3,9-bis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 864448-29-3
3,9-dibenzyl-7-(phenylsulfonyl)-3,7,9-triazabicyclo[3.3.1]nonane

: 864448-31-7
3,9-dibenzyl-3,7,9-triazabicyclo[3.3.1]nonane

Guidance literature:: 3,9-dibenzyl-7-(phenylsulfonyl)-3,7,9-triazabicyclo[3.3.1]nonane; With sodium bis(2-methoxyethoxy)aluminium dihydride; In toluene; xylene; for 1h; Heating / reflux;

With sodium hydroxide; water; In toluene; xylene;

Reference yield: 100.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 864448-31-7
3,9-dibenzyl-3,7,9-triazabicyclo[3.3.1]nonane

: 864448-32-8
3,9-dibenzyl-7-methyl-3,7,9-triazabicyclo[3.3.1]nonane

Guidance literature:: formaldehyd; 3,9-dibenzyl-3,7,9-triazabicyclo[3.3.1]nonane; In methanol; water; at 50 ℃; for 0.25h;

With methanol; sodium tetrahydroborate; water; for 0.25h;

With hydrogenchloride; potassium carbonate; more than 3 stages;

Reference yield:

: 864448-31-7
3,9-dibenzyl-3,7,9-triazabicyclo[3.3.1]nonane

: 868407-52-7
(E)-9-[3-(2-amino-4-chlorophenyl)-acryloyl]-7-(4-fluorobenzyl)-3,7,9-triazabicyclo[3.3.1]nonane-3-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: tert-butyl methyl ether / 0.17 h / 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 4 h / 20 °C / 760.05 Torr

3: sodium hydrogencarbonate / ethanol / 2 h / Heating / reflux

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C

5: sodium hydroxide; ethanol; water / 1.5 h / Heating / reflux

With sodium hydroxide; ethanol; water; hydrogen; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In ethanol; dichloromethane; tert-butyl methyl ether;