Brickellin

Base Information

Chemical Name:Brickellin
CAS No.:90357-63-4
Molecular Formula:C₂₀H₂₀O₉
Molecular Weight:404.373
Hs Code.:
UNII:MQ8CVA2BQ4
ChEMBL ID:CHEMBL484666
DSSTox Substance ID:DTXSID50551638
Metabolomics Workbench ID:26145
Wikidata:Q4965995
Wikipedia:Brickellin

Synonyms:brickellin;MQ8CVA2BQ4;UNII-MQ8CVA2BQ4;90357-63-4;4H-1-Benzopyran-4-one, 5-hydroxy-2-(2-hydroxy-4,5-dimethoxyphenyl)-3,6,7-trimethoxy-;5-Hydroxy-2-(2-hydroxy-4,5-dimethoxyphenyl)-3,6,7-trimethoxy-4H-1-benzopyran-4-one;CHEMBL484666;DTXSID50551638;LMPK12113062;5,2'-dihydroxy-3,6,7,4',5'-penta-methoxyflavone;Q4965995

Suppliers and Price of Brickellin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Brickellin

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:6
Exact Mass:404.11073221
Heavy Atom Count:29
Complexity:621

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)C2=C(C(=O)C3=C(C(=C(C=C3O2)OC)OC)O)OC)O)OC

Technology Process of Brickellin

There total 6 articles about Brickellin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97745-08-9
2'-isopropyloxy-3,5,6,7,4',5'-hexamethoxyflavone

: 90357-63-4
2',5-dihydroxy-3,4',5',6,7-pentamethoxyflavone brickellin

Guidance literature:: With boron trichloride; In dichloromethane; at -60 ℃;
DOI:10.1016/S0031-9422(00)81135-8

Reference yield:

: 22248-14-2
6-hydroxy-2,3,4-trimethoxyacetophenone

: 90357-63-4
2',5-dihydroxy-3,4',5',6,7-pentamethoxyflavone brickellin

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxyde

2: 0.8 g / 35percent H₂O₂, 10percent potassium hydroxide / methanol / 0.25 h / Ambient temperature

3: 200 mg / KOH

4: boron trichloride / CH₂Cl₂ / -60 °C

With potassium hydroxide; dihydrogen peroxide; boron trichloride; In methanol; dichloromethane;
DOI:10.1016/S0031-9422(00)81135-8

Reference yield:

: 97745-09-0
3-hydroxy-2'-isopropyloxy-4',5,5',6,7-pentamethoxyflavone

: 90357-63-4
2',5-dihydroxy-3,4',5',6,7-pentamethoxyflavone brickellin

Guidance literature:: Multi-step reaction with 2 steps

1: 200 mg / KOH

2: boron trichloride / CH₂Cl₂ / -60 °C

With potassium hydroxide; boron trichloride; In dichloromethane;
DOI:10.1016/S0031-9422(00)81135-8