Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl -

Base Information

Chemical Name:Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl -
CAS No.:86515-55-1
Molecular Formula:C47H86O9
Molecular Weight:795.194
Hs Code.:

Synonyms:

Suppliers and Price of Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl -

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl -

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl -

There total 10 articles about Benzenedodecanoic acid, a-(1-hydroxydocosyl)-3,4-dimethoxy-2,5-bis(methoxymethoxy)-6-methyl - which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.9%

: 96012-42-9
ethyl 2-<10-<3,4-dimethoxy-2,5-di(methoxymethoxy)-6-methylphenyl>decyl>-3-hydroxytetracosanoate

: 86515-55-1
2-<10-<3,4-dimethoxy-2,5-di(methoxymethoxy)-6-methylphenyl>decyl>-3-hydroxytetracosanoic acid

Guidance literature:: With sodium hydroxide; In 1,4-dioxane; ethanol; for 2h; Heating;
DOI:10.1246/bcsj.57.3182

Reference yield:

: 96012-47-4
ethyl 2-ethoxycarbonyl-3-oxotetracosanoate

: 86515-55-1
2-<10-<3,4-dimethoxy-2,5-di(methoxymethoxy)-6-methylphenyl>decyl>-3-hydroxytetracosanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 45.2 percent / p-tolunesulfonic acid / dimethylsulfoxide / 0.33 h / 200 - 210 °C

2: 65.6 percent / piperidine, AcOH / benzene / Heating

3: H₂ / Pd black / ethanol; dioxane / 8 h / Ambient temperature

4: 16.9 g / NaBH₄ / methanol; dioxane / 0.5 h

5: 89.9 percent / 3M aq.NaOH / ethanol; dioxane / 2 h / Heating

With piperidine; sodium hydroxide; sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; acetic acid; palladium; In 1,4-dioxane; methanol; ethanol; dimethyl sulfoxide; benzene;
DOI:10.1246/bcsj.57.3182

Reference yield:

: Acetic acid 10-(3,4-dimethoxy-2,5-bis-methoxymethoxy-6-methyl-phenyl)-decyl ester

: 86515-55-1
2-<10-<3,4-dimethoxy-2,5-di(methoxymethoxy)-6-methylphenyl>decyl>-3-hydroxytetracosanoic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 27.4 g / 4M aq.NaOH / ethanol / 15 h / Ambient temperature

2: 81.1 percent / pyridine*SO₃, DMSO, Et₃N / 1 h / Ambient temperature

3: 65.6 percent / piperidine, AcOH / benzene / Heating

4: H₂ / Pd black / ethanol; dioxane / 8 h / Ambient temperature

5: 16.9 g / NaBH₄ / methanol; dioxane / 0.5 h

6: 89.9 percent / 3M aq.NaOH / ethanol; dioxane / 2 h / Heating

With piperidine; sodium hydroxide; sodium tetrahydroborate; hydrogen; sulfur trioxide pyridine complex; acetic acid; dimethyl sulfoxide; triethylamine; palladium; In 1,4-dioxane; methanol; ethanol; benzene;
DOI:10.1246/bcsj.57.3182