Technology Process of 4-Ethynyl-3,6-dimethylpyridazine
There total 2 articles about 4-Ethynyl-3,6-dimethylpyridazine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
methanol;
for 1h;
Ambient temperature;
DOI:10.1055/s-1983-30319
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 88 percent / bispalladium dichloride, copper(I) iodide, triethylamine / 12 h / 100 °C
2: 84 percent / aq. KOH / methanol / 1 h / Ambient temperature
With
bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide; copper(l) iodide; triethylamine;
In
methanol;
DOI:10.1055/s-1983-30319
- Guidance literature:
-
With
sulfuric acid; water; mercury(II) sulfate;
In
acetone;
for 2h;
Heating;
DOI:10.1055/s-1984-30792