5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one

Base Information

Chemical Name:5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one
CAS No.:86532-06-1
Molecular Formula:C₁₂H₁₈O₂
Molecular Weight:194.274
Hs Code.:
DSSTox Substance ID:DTXSID60563207

Synonyms:5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one;86532-06-1;DTXSID60563207;AKOS015908342;5-methyl-5-(4-methyl-1-cyclohex-3-enyl)-tetrahydro-furan-2-one;5-methyl-5-(4-methyl-3-cyclohexen-1-yl)dihydro-2(3H)-furanone

Suppliers and Price of 5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:194.130679813
Heavy Atom Count:14
Complexity:280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CCC(CC1)C2(CCC(=O)O2)C

Technology Process of 5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one

There total 13 articles about 5-Methyl-5-(4-methylcyclohex-3-en-1-yl)oxolan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 96160-48-4
2-(4-Methyl-cyclohex-3-enyl)-hex-5-en-2-ol

: 86532-06-1
rac-Norbisabolid

Guidance literature:: With molecular sieve; pyridinium chlorochromate; In dichloromethane; at 35 - 40 ℃; for 35h;

Reference yield:

: 88153-58-6,132339-35-6
bisabola-2,11-diene-7α,10-diol

: 55169-27-2,63323-23-9,86532-06-1,106862-44-6,106862-45-7
(R)-5-Methyl-5-(4-methyl-cyclohex-3-enyl)-dihydro-furan-2-one

Guidance literature:: With dipyridinium dichromate; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1016/0031-9422(90)80187-L

Reference yield:

: 515-69-5,23089-26-1,23178-88-3,25428-43-7,72059-10-0,72691-24-8,76738-75-5,78148-59-1,123877-54-3,26560-22-5
(-)-α-bisabolol

: 55169-27-2,63323-23-9,86532-06-1,106862-44-6,106862-45-7
(R)-5-Methyl-5-(4-methyl-cyclohex-3-enyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1) O₂, Rose Bengal, 2) NaBH₄ / 1) iso-PrOH, sunlight, 30 min., 2) MeOH, r.t., 1 h

2: 15 mg / pyridinium dichromate / CH₂Cl₂ / 20 h / Ambient temperature

With sodium tetrahydroborate; dipyridinium dichromate; oxygen; rose bengal; In dichloromethane;
DOI:10.1016/0031-9422(90)80187-L