Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester

Base Information

Chemical Name:Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester
CAS No.:870177-36-9
Molecular Formula:C52H93NO23
Molecular Weight:1100.3
Hs Code.:

Benzoic acid,
4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11-
tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester

Synonyms:

Suppliers and Price of Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester

There total 7 articles about Benzoic acid, 4-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-3,5-bis[[1-(2,5,8,11- tetraoxadodec-1-yl)-3,6,9,12-tetraoxatridec-1-yl]oxy]-, 2-propenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

: 870177-17-6
4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoic acid

: 106-95-6
allyl bromide

: 870177-36-9
allyl 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: With tetra-(n-butyl)ammonium iodide; potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1002/chem.200401078

Reference yield:

: 870177-06-3
ethyl 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(benzyloxy)benzoate

: 870177-36-9
allyl 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / Pd/C / methanol / 1 h

2: 65 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

3: 98 percent / aq. KOH / ethanol / 12 h / 20 °C

4: 98.5 percent / K₂CO₃; Bu₄NI / dimethylformamide / 12 h / 20 °C

With potassium hydroxide; hydrogen; tetra-(n-butyl)ammonium iodide; potassium carbonate; palladium on activated charcoal; In methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200401078

Reference yield:

: 831-61-8
Ethyl gallate

: 870177-36-9
allyl 4-(3-tert-butoxycarbonylaminopropoxy)-3,5-bis(1,3-bis{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}propan-2-yloxy)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / KHCO₃; KI / dimethylformamide / 96 h / 20 °C

2: 65 percent / K₂CO₃ / dimethylformamide / 72 h / 80 °C

3: 98 percent / aq. KOH / ethanol / 12 h / 20 °C

4: 98.5 percent / K₂CO₃; Bu₄NI / dimethylformamide / 12 h / 20 °C

With potassium hydroxide; tetra-(n-butyl)ammonium iodide; potassium carbonate; potassium hydrogencarbonate; potassium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.200401078