Technology Process of 2,5-Hexanediamine,
2,5-dimethyl-N,N'-bis(2-methyl-1-phenylpropyl)-N,N'-bis(1-phenylethoxy
)-
There total 8 articles about 2,5-Hexanediamine,
2,5-dimethyl-N,N'-bis(2-methyl-1-phenylpropyl)-N,N'-bis(1-phenylethoxy
)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
Jacobsen catalyst (R,R);
In
ethanol; toluene;
DOI:10.1021/ma051217m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92 percent / Cu(OAc)2; aq. NH4OH / methanol; ethanol; propan-2-ol
2: 43 percent / NaBH4 / Jacobsen catalyst (R,R) / toluene; ethanol
With
ammonium hydroxide; sodium tetrahydroborate; copper diacetate;
Jacobsen catalyst (R,R);
In
methanol; ethanol; isopropyl alcohol; toluene;
DOI:10.1021/ma051217m
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 67 percent / thiourea; glacial AcOH / ethanol / Heating
2: 89 percent / 4 Angstroem molecular sieves / tetrahydrofuran / Heating
3: 44 percent / Na2CO3; m-chloroperbenzoic acid / CHCl3 / 20 °C
4: 54 percent / acetonitrile / 72 h / Heating
5: 72 percent / 1,4-diazabicyclo[2.2.2]octane; Me3SiCl / tetrahydrofuran / 3.5 h / 0 - 20 °C
6: 92 percent / Cu(OAc)2; aq. NH4OH / methanol; ethanol; propan-2-ol
7: 43 percent / NaBH4 / Jacobsen catalyst (R,R) / toluene; ethanol
With
1,4-diaza-bicyclo[2.2.2]octane; ammonium hydroxide; sodium tetrahydroborate; chloro-trimethyl-silane; copper diacetate; 4 A molecular sieve; sodium carbonate; acetic acid; thiourea; 3-chloro-benzenecarboperoxoic acid;
Jacobsen catalyst (R,R);
In
tetrahydrofuran; methanol; ethanol; chloroform; isopropyl alcohol; toluene; acetonitrile;
DOI:10.1021/ma051217m