Technology Process of lithium S-{2-[(3-amino-3-thioxopropyl)amino]ethyl} hydrogen thiophosphate
There total 6 articles about lithium S-{2-[(3-amino-3-thioxopropyl)amino]ethyl} hydrogen thiophosphate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium thiophosphate powder;
In
water; N,N-dimethyl-formamide;
for 2.75h;
DOI:10.1021/jm00171a026
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 77 percent / NaH (50percent oil suspension) / dimethylformamide
2: 54 percent / Lawesson's reagent / tetrahydrofuran / 2 h
3: 64 percent / acetic acid, HBr / Ambient temperature
4: 65 percent / Li3SPO3*4.2H2O / H2O; dimethylformamide / 2.75 h
With
Lawessons reagent; lithium thiophosphate powder; hydrogen bromide; sodium hydride; acetic acid;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00171a026
- Guidance literature:
-
Multi-step reaction with 6 steps
1: SOCl2 / CHCl3 / 1 h / Heating
2: 60 percent / NH3 / tetrahydrofuran
3: 77 percent / NaH (50percent oil suspension) / dimethylformamide
4: 54 percent / Lawesson's reagent / tetrahydrofuran / 2 h
5: 64 percent / acetic acid, HBr / Ambient temperature
6: 65 percent / Li3SPO3*4.2H2O / H2O; dimethylformamide / 2.75 h
With
Lawessons reagent; thionyl chloride; lithium thiophosphate powder; ammonia; hydrogen bromide; sodium hydride; acetic acid;
In
tetrahydrofuran; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00171a026
