Technology Process of L-Tryptophanamide,
1-[(1,1-dimethylethoxy)carbonyl]-N-[(phenylmethoxy)carbonyl]-L-tryptoph
yl-N-[11-(2-carboxyethyl)-1,5-dioxaspiro[5.5]undec-7-yl]-1-[(1,1-dimethyl
ethoxy)carbonyl]-
There total 1 articles about L-Tryptophanamide,
1-[(1,1-dimethylethoxy)carbonyl]-N-[(phenylmethoxy)carbonyl]-L-tryptoph
yl-N-[11-(2-carboxyethyl)-1,5-dioxaspiro[5.5]undec-7-yl]-1-[(1,1-dimethyl
ethoxy)carbonyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium permanganate; sodium periodate; sodium hydrogencarbonate;
In
acetone;
at 20 ℃;
for 6h;
DOI:10.1021/jm050488k
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 50 ℃;
for 4h;
DOI:10.1021/jm050488k
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
N,N-dimethyl-formamide;
at 50 ℃;
DOI:10.1021/jm050488k