4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate

Base Information

Chemical Name:4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate
CAS No.:870637-61-9
Molecular Formula:C12H11ClO5S
Molecular Weight:302.735
Hs Code.:
DSSTox Substance ID:DTXSID00469411
Wikidata:Q82297122

Synonyms:4-[4-(CHLOROSULFONYL)PHENOXY]-2-BUTYNYL ACETATE;870637-61-9;SCHEMBL5661150;DTXSID00469411;UNMLQVHKQGNATN-UHFFFAOYSA-N

Suppliers and Price of 4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:302.0015723
Heavy Atom Count:19
Complexity:459

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OCC#CCOC1=CC=C(C=C1)S(=O)(=O)Cl

Technology Process of 4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate

There total 2 articles about 4-[4-(Chlorosulfonyl)phenoxy]-2-butynyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 870637-63-1
4-(4-acetoxy-but-2-ynyloxy)-benzenesulfonic acid sodium salt

: 870637-61-9
4-[4-(chlorosulfonyl)phenoxy]-2-butynyl acetate

Guidance literature:: With oxalyl dichloride; water; N,N-dimethyl-formamide; In dichloromethane; at 10 - 23 ℃; for 2.16667h; Product distribution / selectivity;

Reference yield: 55.0%

: 15779-55-2
acetic acid-(4-phenoxy-but-2-ynyl ester)

: 870637-61-9
4-[4-(chlorosulfonyl)phenoxy]-2-butynyl acetate

Guidance literature:: acetic acid-(4-phenoxy-but-2-ynyl ester); With chlorosulfonic acid; In dichloromethane; at -5 - 22 ℃; for 1 - 2h;

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 19 - 20h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 870637-61-9
4-[4-(chlorosulfonyl)phenoxy]-2-butynyl acetate

: 84915-43-5
(3S)-2,2-dimethyl-tetrahydro-2H-1,4-thiazine-3-carboxylic acid

: C₁₉H₂₂ClNO₆S₂

Guidance literature:: (3S)-2,2-dimethyl-tetrahydro-2H-1,4-thiazine-3-carboxylic acid; With N,O-Bis(trimethylsilyl)trifluoroacetamide; In dichloromethane; at 40 - 41 ℃; for 1.5 - 2.5h; Heating / reflux;

With 4-methyl-morpholine; In dichloromethane; at 5 - 10 ℃; for 0.0833333 - 0.166667h;

4-[4-(chlorosulfonyl)phenoxy]-2-butynyl acetate; With oxalyl dichloride; N,N-dimethyl-formamide; more than 3 stages;