Technology Process of Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-
There total 6 articles about Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
toluene;
Yields of byproduct given;
Heating;
DOI:10.3987/COM-94-6744
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / PPh3, Et3N, PdCl2, CuI / dimethylformamide / 0.5 h / 85 °C
2: H2 / Raney Ni / methanol / 20 °C
3: 81 percent / TsOH*H2O / toluene / Heating
With
copper(l) iodide; hydrogen; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; palladium dichloride;
nickel;
In
methanol; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-94-6744
- Guidance literature:
-
Multi-step reaction with 4 steps
1: I2, CF3CO2Ag / CHCl3 / Ambient temperature
2: 90 percent / PPh3, Et3N, PdCl2, CuI / dimethylformamide / 0.5 h / 85 °C
3: H2 / Raney Ni / methanol / 20 °C
4: 81 percent / TsOH*H2O / toluene / Heating
With
copper(l) iodide; hydrogen; iodine; silver trifluoroacetate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; palladium dichloride;
nickel;
In
methanol; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-94-6744