Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-

Base Information

Chemical Name:Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-
CAS No.:87080-11-3
Molecular Formula:C15H20O3
Molecular Weight:248.322
Hs Code.:
DSSTox Substance ID:DTXSID90560860

Synonyms:87080-11-3;DTXSID90560860;1-[2,4-Dimethoxy-5-(3-methylbut-2-en-1-yl)phenyl]ethan-1-one

Suppliers and Price of Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:248.14124450
Heavy Atom Count:18
Complexity:305

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCC1=CC(=C(C=C1OC)OC)C(=O)C)C

Technology Process of Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]-

There total 6 articles about Ethanone, 1-[2,4-dimethoxy-5-(3-methyl-2-butenyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1-[5-(3-Hydroxy-3-methyl-butyl)-2,4-dimethoxy-phenyl]-ethanone

: 87080-11-3
2,4-Dimethoxy-5-C-prenylacetophenone

: 1-[2,4-Dimethoxy-5-(3-methyl-but-3-enyl)-phenyl]-ethanone

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Yields of byproduct given; Heating;
DOI:10.3987/COM-94-6744

Reference yield:

: 3153-75-1
1-(5-iodo-2,4-dimethoxyphenyl)ethan-1-one

: 87080-11-3
2,4-Dimethoxy-5-C-prenylacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / PPh₃, Et₃N, PdCl₂, CuI / dimethylformamide / 0.5 h / 85 °C

2: H₂ / Raney Ni / methanol / 20 °C

3: 81 percent / TsOH*H₂O / toluene / Heating

With copper(l) iodide; hydrogen; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; palladium dichloride; nickel; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-94-6744

Reference yield:

: 829-20-9
2',4'-dimethoxyacetophenone

: 87080-11-3
2,4-Dimethoxy-5-C-prenylacetophenone

Guidance literature:: Multi-step reaction with 4 steps

1: I₂, CF₃CO₂Ag / CHCl₃ / Ambient temperature

2: 90 percent / PPh₃, Et₃N, PdCl₂, CuI / dimethylformamide / 0.5 h / 85 °C

3: H₂ / Raney Ni / methanol / 20 °C

4: 81 percent / TsOH*H₂O / toluene / Heating

With copper(l) iodide; hydrogen; iodine; silver trifluoroacetate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; palladium dichloride; nickel; In methanol; chloroform; N,N-dimethyl-formamide; toluene;
DOI:10.3987/COM-94-6744