3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione

Base Information

Chemical Name:3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione
CAS No.:87239-97-2
Molecular Formula:C₁₀H₈N₄S₂
Molecular Weight:248.332
Hs Code.:
DSSTox Substance ID:DTXSID50554447
Wikidata:Q82435443

Synonyms:87239-97-2;DTXSID50554447;3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione

Suppliers and Price of 3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:248.01903862
Heavy Atom Count:16
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C2=NN=C3N2NC(=S)S3

Technology Process of 3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione

There total 3 articles about 3-(2-Methylphenyl)[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole-6(5H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 75-15-0,12122-00-8
carbon disulfide

: 87239-95-0
4-amino-5-(2-methylphenyl)-4H-1,2,4-triazole-3-thiol

: 87239-97-2
3-(2-Tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazol-6(5H)-thione

Guidance literature:: With pyridine; at 100 ℃;

Reference yield: 48.0%

: 75-15-0,12122-00-8
carbon disulfide

: 87239-95-0
4-amino-2,4-dihydro-5-(2-methylphenyl)-3H-1,2,4-triazole-3-thione

: 87239-97-2
3-(2-Tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazol-6(5H)-thione

Guidance literature:: With potassium hydroxide; In methanol; for 24h; Heating;

Reference yield:

: 7658-80-2
2-methylbenzohydrazide

: 87239-97-2
3-(2-Tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazol-6(5H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / KOH, NH₂NH₂*H₂O

2: 58 percent / pyridine / 100 °C

With pyridine; potassium hydroxide; hydrazine hydrate;