(2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide

Base Information

Chemical Name:(2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide
CAS No.:586-02-7
Molecular Formula:C₄₈H₉₃NO₉
Molecular Weight:828.268
Hs Code.:

Synonyms:(R)-2-hydroxy-tetracosanoic acid-((1S,2R)-1-β-D-galactopyranosyloximethyl-2-hydroxy-heptadec-3t-enylamide);(R)-2-Hydroxy-tetracosansaeure-((1S,2R)-1-β-D-galactopyranosyloxymethyl-2-hydroxy-heptadec-3t-enylamid);(R)-2-Hydroxy-tetracosanoic acid [(E)-(1S,2R)-2-hydroxy-1-((2R,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-heptadec-3-enyl]-amide;

Suppliers and Price of (2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PHRENOSIN 95.00%
5MG
$ 498.20

Total 6 raw suppliers

Chemical Property of (2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:923.1°Cat760mmHg
Flash Point:512.1°C
PSA：168.94000
Density:1.05g/cm³
LogP:9.86970

Purity/Quality:

99% ^*data from raw suppliers

PHRENOSIN 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide

There total 3 articles about (2S)-N-[(1S,2R,3E)-1-[(β-D-Galactopyranosyloxy)methyl]-2-hydroxy-3-heptadecenyl]-2-hydroxytetracosanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108041-03-8
Acetic acid (2R,3S,4S,5R,6R)-3,5-diacetoxy-2-acetoxymethyl-6-[(E)-(2S,3R)-3-hydroxy-2-((R)-2-hydroxy-tetracosanoylamino)-octadec-4-enyloxy]-tetrahydro-pyran-4-yl ester

: 586-02-7
(2S,3R,4E)-1-O-β-D-galactopyranosyl-N-(2'R)-2'-hydroxytetracosanoylsphingenine

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 4h; Yield given;
DOI:10.1016/0008-6215(87)80219-7

Reference yield:

: 112146-64-2,112246-62-5
(2S,3R,4E)-N-(2'R)-2'-tert-butyldiphenylsilyloxytetracosanoyl-1-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)sphingenine

: 586-02-7
(2S,3R,4E)-1-O-β-D-galactopyranosyl-N-(2'R)-2'-hydroxytetracosanoylsphingenine

Guidance literature:: Multi-step reaction with 2 steps

1: M Bu₄NF / tetrahydrofuran / 0.5 h / 20 °C

2: NaOMe / methanol / 4 h / 20 °C

With tetrabutyl ammonium fluoride; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1016/0008-6215(87)80219-7

Reference yield:

: 586-02-7,33037-13-7,112246-64-7,136598-19-1
N-Cerebronyl-1-D-erythro-sphingosyl-β-D-galaktopyranosid , Phrenosin

Guidance literature:: Duch Verseifung d. entspr. 3-O-Benzoyl-penta-O-acetyl-galaktosids in abs. Me. , bei Ggw. einer Spur NaOCH3 bei 35-40grad;
DOI:10.1021/ja01476a033